Synthesis in the diazasteroid group. I. A new synthesis of 8,13-diaza-2,3-dimethoxygona-1,3,5(10)triene and its mercuric acetate oxidation |
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| Authors: | Katsuhide Matoba Kazumasa Isomura Masanori Nagata Takao Yamazaki Raymond N Castle |
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| Abstract: | From the condensation reaction of methyl butyrolactim (I) with 1-ethoxycarbonylmethyl-6,7-dimethoxy-l,2,3,4-tetrahydroisoquinoline (II), 8,13-diaza-2,3-dimethoxygona-l,3,5(10)trien-12-one (VI) and 8,13-diaza-2,3-dimethoxygona-l,3,5(10)triene (VII) were obtained in good yield. The oxidation of VI and VII with mercuric acetate was examined. |
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