Thermal and microwave-assisted N-formylation using solid-supported reagents |
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Authors: | Bimbisar Desai Timothy N. Danks Gabriele Wagner |
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Affiliation: | a Chemistry Division, SBMS, University of Surrey, Guildford, Surrey GU2 7XH, UK b The Oratory School, Woodcote, Reading RG8 0PJ, UK |
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Abstract: | A rapid and easy route to formamides by microwave assisted N-formylation of primary and secondary amines is described. Using an insoluble polymer or an inorganic solid-supported reagent as a formylating agent, microwave irradiation furnished the corresponding formamides in high yields, with reduced reaction time and solvent volume over the conventional approach. |
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Keywords: | Formamides Microwave irradiation Solid-supported formate |
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