| 高效液相色谱-串联质谱法测定动物源性食品中20种磺酰脲类除草剂残留 |
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| 引用本文： | 刘锦霞,张莹,丁利,刘晓霞,黄志强,陈波,王利兵. 高效液相色谱-串联质谱法测定动物源性食品中20种磺酰脲类除草剂残留[J]. 分析化学, 2011, 39(5): 664-669. DOI: 10.3724/SP.J.1096.2011.00664 |
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| 作者姓名： | 刘锦霞 张莹 丁利 刘晓霞 黄志强 陈波 王利兵 |
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| 作者单位： | 刘锦霞,刘晓霞,LIU Jin-Xia,LIU Xiao-Xia(湖南省检验检疫科学技术研究院,湖南出入境检验检疫局技术中心,食品安全科学技术湖南省重点实验室,长沙,410004;湖南师范大学,化学生物学及中药分析省部共建教育部重点实验室,长沙,410081);张莹,丁利,黄志强,王利兵,ZHANG Yi,DING Li,HUANG Zhi-Qiang,WANG Li-Bing(湖南省检验检疫科学技术研究院,湖南出入境检验检疫局技术中心,食品安全科学技术湖南省重点实验室,长沙,410004);陈波,CHEN Bo(湖南师范大学化学生物学及中药分析省部共建教育部重点实验室,长沙,410081) |
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| 基金项目： | 湖南省科技专项湖南省食品安全监控技术体系研究与示范基金，国家公益性项目基金 |
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| 摘 要： | 建立了动物源性食品中20种磺酰脲类除草剂多残留的分析方法.样品经乙腈均质提取2次,经Waters Oasis HLB固相萃取小柱净化后,在高效液相色谱-电喷雾串联质谱仪多反应监测模式下测定,采用质谱法定性,外标法定量.除草剂采用Eclipse AAA色谱柱,以甲醇和0.1%乙酸溶液为流动相,在梯度洗脱条件下可以得到很好...
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| 关 键 词： | 高效液相色谱-串联质谱 磺酰脲类除草剂 动物源性食品 |
Determination of 20 Sulfonylurea Herbicides Residues in Animal Origin Foods by High Performance Liquid Chromatography-Tandem Mass Spectrometry |
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| LIU Jin-Xia,ZHANG Yi,DING Li,LIU Xiao-Xia,HUANG Zhi-Qiang,CHEN Bo,WANG Li-Bing. Determination of 20 Sulfonylurea Herbicides Residues in Animal Origin Foods by High Performance Liquid Chromatography-Tandem Mass Spectrometry[J]. Chinese Journal of Analytical Chemistry, 2011, 39(5): 664-669. DOI: 10.3724/SP.J.1096.2011.00664 |
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| Authors: | LIU Jin-Xia ZHANG Yi DING Li LIU Xiao-Xia HUANG Zhi-Qiang CHEN Bo WANG Li-Bing |
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| Affiliation: | LIU Jin-Xia1,2,ZHANG Yi1,DING Li1,LIU Xiao-Xia1,HUANG Zhi-Qiang1,CHEN Bo2,WANG Li-Bing2 1(Hunan Academy of Inspection and Quarantine,Technology Center of Hunan Entry-Exit Inspection and Quarantine Bureau,Hunan Key Laboratory of Food Safety Science & Technology,Changsha 410004) 2(Hunan Normal University,Key laboratory of Chemical Biology & Traditional Chinese Medicine Research,Ministry of Education,Changsha 410081) |
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| Abstract: | A method was developed for the determination of 20 sulfonylurea herbicides residues in animal origin foods by high performance liquid chromatographytandem mass spectrometry(LC-MS/MS).Sulfonylurea herbicides were extracted with acetonitrile and the extract was cleaned up by Waters Oasis HLB solid phase extraction column.Qualitation of the analytes was achieved with multiple reaction monitoring(MRM) and external standard method was used for quantification.The chromatography separation was achieved in gradient... |
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| Keywords: | High performance liquid chromatographytandem mass spectrometry Sulfonylurea herbicides Animal-derived food |
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