Thermoanalytical investigation of crystallin cerium phosphate |
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Authors: | L Zsinka L Szirtes Le Van So Z Pokó |
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Institution: | (1) Institute of Isotopes of the Hungarian Academy of Sciences, PO Box 77, H-1525 Budapest;(2) Central Research Institute for Physics of the Hungarian Academy of Sciences, PO Box 49, H-1525 Budapest, Hungary |
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Abstract: | The crystalline cerium bis-monohydrogen phosphate Ce(HPO4)2·1.33 H2O was synthetized and identified by X-ray and analytical methods.The thermal decomposition was investigated by simultaneous TG, DTG and DTA measurements. As a result of investigations four endothermic processes with weight loss were found; the first two, nearly equal peaks at 373 and 423 K, the third at 653 K and the last at 1053 K. The material after heating over 1273 K was investigated with the same analytical methods. In connection with these data we supposed that the weight losses may be identified as water and oxigen losses. The thermal analysis was supported by X-ray measurements. Collecting the results of thermal and X-ray analysis crystalline water bound in the molecule in various ways can be quantitatively distinguished. It was found that this phenomena have definite influence on the layer distance.By the X-ray measurements the change of the crystal structure taking place during the heating process could be followed.
Zusammenfassung Das kristalline Cer-bis-phosphat Ce(HPO4)2.1.33 H2O] wurde synthetisiert und durch Röntgen- und analytische Methoden identifiziert.Die thermische Zersetzung wurde durch simultane TG-, DTG- und DTA-Messungen untersucht. Als Ergebnis der Untersuchungen wurden vier endotherme Vorgänge mit Gewichtsverlust gefunden: die ersten zwei annähernd gleichen Peaks bei 373 und 423 K, der Dritte bei 635 K und der Letzte bei 1053 K. Nach Erhitzen über 1273 K wurde die Substanz mit den gleichen analytischen Methoden untersucht. Im Zusammenhang mit diesen Angaben wurde angenommen, dass die Gewichtsverluste der Abgabe von Wasser und Sauerstoff zugeordnet werden können. Die Thermoanalyse wurde durch Röntgenuntersuchungen unterstützt. Durch gemeinsame Auswertung der Ergebnisse der Thermo- und Röntgenanalyse konnte das im Molekül auf verschiedene Arte gebundene Kristallwasser quantitativ unterschieden werden. Es wurde gefunden, dass dieses Phänomen einen ausgeprägten Einfluss auf den Abstand der Schichtenentfernung hat.Durch Röntgenmessungen konnten die während des Aufheizvorganges stattfindenden Veränderungen der Kristallstruktur verfolgt werden.
Résumé Le bis(monohydrogéno)phosphate de cérium Ce(HPO4)2.1,33 H2O] cristallin a été synthétisé et identifié par les méthodes analytiques et par rayons X.La décomposition thermique a été suivie par TG, TGD et ATD simultanées. Les résultats des essais ont mis en évidence quatre processus endothermiques avec perte de poids: les deux premiers, avec des pics sensiblement égaux à 373 et 423 K, le troisième à 653 K et le dernier à 1053 K. AprÊs chauffage au-dessus de 1273 K le matériau a été étudié à l'aide des mèmes méthodes analytiques. D'aprÊs ces données, les pertes de poids peuvent sans doute Être attribuées à des pertes d'eau et d'oxygÊne. L'analyse thermique a été étayée par examen aux rayons X. Le rapprochement des résultats a permis de distinguer de faÇon quantitative divers modes de liaison de l'eau de cristallisation dans la molécule. On établit que ce phénomène a une influence définie sur la distance des couches.Les mesures aux rayons X ont permis de suivre le changement de la structure cristalline pendant le chauffage.
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2
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![kcy](/content/tmk111373808x895/xxlarge1082.gif) , ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Mcy](/content/tmk111373808x895/xxlarge1052.gif) ![pcy](/content/tmk111373808x895/xxlarge1087.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Ucy](/content/tmk111373808x895/xxlarge1059.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) 373 423 , ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) — ![pcy](/content/tmk111373808x895/xxlarge1087.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) 653 ![pcy](/content/tmk111373808x895/xxlarge1087.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Dcy](/content/tmk111373808x895/xxlarge1044.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) — ![pcy](/content/tmk111373808x895/xxlarge1087.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) 1053 . ![IOcy](/content/tmk111373808x895/xxlarge1025.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Dcy](/content/tmk111373808x895/xxlarge1044.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![pcy](/content/tmk111373808x895/xxlarge1087.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![gcy](/content/tmk111373808x895/xxlarge1075.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Vcy](/content/tmk111373808x895/xxlarge1042.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![Vcy](/content/tmk111373808x895/xxlarge1042.gif) ![ycy](/content/tmk111373808x895/xxlarge1099.gif) 1273 ![Bcy](/content/tmk111373808x895/xxlarge1041.gif) ![ycy](/content/tmk111373808x895/xxlarge1099.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Dcy](/content/tmk111373808x895/xxlarge1044.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![Vcy](/content/tmk111373808x895/xxlarge1042.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Mcy](/content/tmk111373808x895/xxlarge1052.gif) ![zhcy](/content/tmk111373808x895/xxlarge1078.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![Mcy](/content/tmk111373808x895/xxlarge1052.gif) ![ycy](/content/tmk111373808x895/xxlarge1099.gif) ![Mcy](/content/tmk111373808x895/xxlarge1052.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![CHcy](/content/tmk111373808x895/xxlarge1063.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![kcy](/content/tmk111373808x895/xxlarge1082.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![Mcy](/content/tmk111373808x895/xxlarge1052.gif) ![Mcy](/content/tmk111373808x895/xxlarge1052.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![Dcy](/content/tmk111373808x895/xxlarge1044.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![Mcy](/content/tmk111373808x895/xxlarge1052.gif) . ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![Vcy](/content/tmk111373808x895/xxlarge1042.gif) ![pcy](/content/tmk111373808x895/xxlarge1087.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Ucy](/content/tmk111373808x895/xxlarge1059.gif) ![CHcy](/content/tmk111373808x895/xxlarge1063.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![ycy](/content/tmk111373808x895/xxlarge1099.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![zhcy](/content/tmk111373808x895/xxlarge1078.gif) ![Ucy](/content/tmk111373808x895/xxlarge1059.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![softcy](/content/tmk111373808x895/xxlarge1100.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![Bcy](/content/tmk111373808x895/xxlarge1041.gif) ![ycy](/content/tmk111373808x895/xxlarge1099.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![pcy](/content/tmk111373808x895/xxlarge1087.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Dcy](/content/tmk111373808x895/xxlarge1044.gif) ![pcy](/content/tmk111373808x895/xxlarge1087.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![zhcy](/content/tmk111373808x895/xxlarge1078.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) , ![CHcy](/content/tmk111373808x895/xxlarge1063.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![pcy](/content/tmk111373808x895/xxlarge1087.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Vcy](/content/tmk111373808x895/xxlarge1042.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![Mcy](/content/tmk111373808x895/xxlarge1052.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![gcy](/content/tmk111373808x895/xxlarge1075.gif) ![Ucy](/content/tmk111373808x895/xxlarge1059.gif) ![Bcy](/content/tmk111373808x895/xxlarge1041.gif) ![ycy](/content/tmk111373808x895/xxlarge1099.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![Dcy](/content/tmk111373808x895/xxlarge1044.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![Fcy](/content/tmk111373808x895/xxlarge1060.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![tscy](/content/tmk111373808x895/xxlarge1094.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![Vcy](/content/tmk111373808x895/xxlarge1042.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![kcy](/content/tmk111373808x895/xxlarge1082.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![pcy](/content/tmk111373808x895/xxlarge1087.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Vcy](/content/tmk111373808x895/xxlarge1042.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![Dcy](/content/tmk111373808x895/xxlarge1044.gif) ![kcy](/content/tmk111373808x895/xxlarge1082.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Dcy](/content/tmk111373808x895/xxlarge1044.gif) . ![Dcy](/content/tmk111373808x895/xxlarge1044.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![ycy](/content/tmk111373808x895/xxlarge1099.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Mcy](/content/tmk111373808x895/xxlarge1052.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![CHcy](/content/tmk111373808x895/xxlarge1063.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![kcy](/content/tmk111373808x895/xxlarge1082.gif) ![gcy](/content/tmk111373808x895/xxlarge1075.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![zhcy](/content/tmk111373808x895/xxlarge1078.gif) ![Bcy](/content/tmk111373808x895/xxlarge1041.gif) ![ycy](/content/tmk111373808x895/xxlarge1099.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![pcy](/content/tmk111373808x895/xxlarge1087.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![Dcy](/content/tmk111373808x895/xxlarge1044.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Vcy](/content/tmk111373808x895/xxlarge1042.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![zhcy](/content/tmk111373808x895/xxlarge1078.gif) ![Dcy](/content/tmk111373808x895/xxlarge1044.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![gcy](/content/tmk111373808x895/xxlarge1075.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![gcy](/content/tmk111373808x895/xxlarge1075.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![Fcy](/content/tmk111373808x895/xxlarge1060.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![CHcy](/content/tmk111373808x895/xxlarge1063.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![kcy](/content/tmk111373808x895/xxlarge1082.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![Mcy](/content/tmk111373808x895/xxlarge1052.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![zhcy](/content/tmk111373808x895/xxlarge1078.gif) ![Mcy](/content/tmk111373808x895/xxlarge1052.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![softcy](/content/tmk111373808x895/xxlarge1100.gif) ![Mcy](/content/tmk111373808x895/xxlarge1052.gif) . ![pcy](/content/tmk111373808x895/xxlarge1087.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Ucy](/content/tmk111373808x895/xxlarge1059.gif) ![CHcy](/content/tmk111373808x895/xxlarge1063.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![ycy](/content/tmk111373808x895/xxlarge1099.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![zhcy](/content/tmk111373808x895/xxlarge1078.gif) ![Ucy](/content/tmk111373808x895/xxlarge1059.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![softcy](/content/tmk111373808x895/xxlarge1100.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Mcy](/content/tmk111373808x895/xxlarge1052.gif) ![CHcy](/content/tmk111373808x895/xxlarge1063.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![kcy](/content/tmk111373808x895/xxlarge1082.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![gcy](/content/tmk111373808x895/xxlarge1075.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![gcy](/content/tmk111373808x895/xxlarge1075.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![gcy](/content/tmk111373808x895/xxlarge1075.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![Fcy](/content/tmk111373808x895/xxlarge1060.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![CHcy](/content/tmk111373808x895/xxlarge1063.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![kcy](/content/tmk111373808x895/xxlarge1082.gif) ![gcy](/content/tmk111373808x895/xxlarge1075.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![zhcy](/content/tmk111373808x895/xxlarge1078.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![pcy](/content/tmk111373808x895/xxlarge1087.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![zhcy](/content/tmk111373808x895/xxlarge1078.gif) ![Vcy](/content/tmk111373808x895/xxlarge1042.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![softcy](/content/tmk111373808x895/xxlarge1100.gif) ![Ucy](/content/tmk111373808x895/xxlarge1059.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![CHcy](/content/tmk111373808x895/xxlarge1063.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Vcy](/content/tmk111373808x895/xxlarge1042.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![zhcy](/content/tmk111373808x895/xxlarge1078.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![kcy](/content/tmk111373808x895/xxlarge1082.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![zhcy](/content/tmk111373808x895/xxlarge1078.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![tscy](/content/tmk111373808x895/xxlarge1094.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Ucy](/content/tmk111373808x895/xxlarge1059.gif) ![Vcy](/content/tmk111373808x895/xxlarge1042.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![Dcy](/content/tmk111373808x895/xxlarge1044.gif) , ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![zhcy](/content/tmk111373808x895/xxlarge1078.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![CHcy](/content/tmk111373808x895/xxlarge1063.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![ycy](/content/tmk111373808x895/xxlarge1099.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![Bcy](/content/tmk111373808x895/xxlarge1041.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![Vcy](/content/tmk111373808x895/xxlarge1042.gif) ![softcy](/content/tmk111373808x895/xxlarge1100.gif) ![zhcy](/content/tmk111373808x895/xxlarge1078.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Ucy](/content/tmk111373808x895/xxlarge1059.gif) ![Mcy](/content/tmk111373808x895/xxlarge1052.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![kcy](/content/tmk111373808x895/xxlarge1082.gif) ![Ucy](/content/tmk111373808x895/xxlarge1059.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) . ![Bcy](/content/tmk111373808x895/xxlarge1041.gif) ![ycy](/content/tmk111373808x895/xxlarge1099.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![Dcy](/content/tmk111373808x895/xxlarge1044.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) , ![CHcy](/content/tmk111373808x895/xxlarge1063.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![IOcy](/content/tmk111373808x895/xxlarge1025.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Vcy](/content/tmk111373808x895/xxlarge1042.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![kcy](/content/tmk111373808x895/xxlarge1082.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![zhcy](/content/tmk111373808x895/xxlarge1078.gif) ![ycy](/content/tmk111373808x895/xxlarge1099.gif) ![Vcy](/content/tmk111373808x895/xxlarge1042.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![pcy](/content/tmk111373808x895/xxlarge1087.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Dcy](/content/tmk111373808x895/xxlarge1044.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![Vcy](/content/tmk111373808x895/xxlarge1042.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![softcy](/content/tmk111373808x895/xxlarge1100.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![softcy](/content/tmk111373808x895/xxlarge1100.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) . ![pcy](/content/tmk111373808x895/xxlarge1087.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![Dcy](/content/tmk111373808x895/xxlarge1044.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![zhcy](/content/tmk111373808x895/xxlarge1078.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![Ucy](/content/tmk111373808x895/xxlarge1059.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![gcy](/content/tmk111373808x895/xxlarge1075.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![gcy](/content/tmk111373808x895/xxlarge1075.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![Fcy](/content/tmk111373808x895/xxlarge1060.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![CHcy](/content/tmk111373808x895/xxlarge1063.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![kcy](/content/tmk111373808x895/xxlarge1082.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Dcy](/content/tmk111373808x895/xxlarge1044.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![Vcy](/content/tmk111373808x895/xxlarge1042.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![zhcy](/content/tmk111373808x895/xxlarge1078.gif) ![Mcy](/content/tmk111373808x895/xxlarge1052.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![kcy](/content/tmk111373808x895/xxlarge1082.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![lcy](/content/tmk111373808x895/xxlarge1083.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![CHcy](/content/tmk111373808x895/xxlarge1063.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![kcy](/content/tmk111373808x895/xxlarge1082.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Ucy](/content/tmk111373808x895/xxlarge1059.gif) ![kcy](/content/tmk111373808x895/xxlarge1082.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![Ucy](/content/tmk111373808x895/xxlarge1059.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) , ![Icy](/content/tmk111373808x895/xxlarge1048.gif) ![Mcy](/content/tmk111373808x895/xxlarge1052.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Ucy](/content/tmk111373808x895/xxlarge1059.gif) ![SHCHcy](/content/tmk111373808x895/xxlarge1065.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Mcy](/content/tmk111373808x895/xxlarge1052.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![tcy](/content/tmk111373808x895/xxlarge1090.gif) ![pcy](/content/tmk111373808x895/xxlarge1087.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![Ocy](/content/tmk111373808x895/xxlarge1054.gif) ![tscy](/content/tmk111373808x895/xxlarge1094.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![scy](/content/tmk111373808x895/xxlarge1089.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![gcy](/content/tmk111373808x895/xxlarge1075.gif) ![Rcy](/content/tmk111373808x895/xxlarge1056.gif) ![IEcy](/content/tmk111373808x895/xxlarge1045.gif) ![Vcy](/content/tmk111373808x895/xxlarge1042.gif) ![Acy](/content/tmk111373808x895/xxlarge1040.gif) ![Ncy](/content/tmk111373808x895/xxlarge1053.gif) ![Icy](/content/tmk111373808x895/xxlarge1048.gif) .
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