Structure and phase composition of the intermetallide Ni3Al+0.5 at.% B synthesized under pressure

We have used x-ray structural analysis, together with transmission and scanning electron microscopy, to study the phase composition, structure, and elemental distribution in the intermetallide Ni₃Al+0.5 at.% B, produced by self-propagating high-temperature synthesis under pressure. It is shown that the synthesized material is an ordered alloy of the type L1₂. The phase composition of the alloy Ni₃Al+0.5 at.% B is represented by the phases Ni₃Al (the fundamental phase), grains of a layered NiAl composition, and inclusions of Ni₃B. The latter is found inside the Ni₃Al grains, in the form of surrounded particles, and at dislocations and at grain boundaries in the NiAl phase. Institute for the Physics of Strength and Materials Production. Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 9, pp. 59–64, September, 1996.