Synthesis and clathrates of oligomeric 2-O-naphthoide macrocycles |
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| Authors: | AlHujran Tayel A Dawe Louise N Collins Julie Georghiou Paris E |
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| Institution: | Department of Chemistry, Memorial University of Newfoundland, St. John's, Canada. |
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| Abstract: | New macrocyclic O-naphthoides 4-6 were synthesized from dehydration reactions of 3-hydroxy- and 7-tert-butyl-3-hydroxy-2-naphthoic acids, respectively. Their X-ray structures were determined and their clathrate inclusion properties were investigated. Hexamer 6 formed an inclusion clathrate with four chloroform molecules. The trimer 5, by analogy with tri-o-thymotide, was studied for its potential optical resolution effects. |
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