| 四溴邻苯二甲酸双酯的固－液相转移催化合成 |
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| 引用本文： | 王筱梅,王西奎,徐广通,孟平蕊.四溴邻苯二甲酸双酯的固－液相转移催化合成[J].应用化学,1995(4). |
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| 作者姓名： | 王筱梅 王西奎 徐广通 孟平蕊 |
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| 作者单位： | 山东建筑材料工业学院应用化学系 |
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| 基金项目： | 国家自然科学基金资助课题 |
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| 摘 要： | 使用固－液相转移催化法合成了１８种标题化合物，产率最高达９３．４％，部分化合物结构由ＩＲ，１ＨＮＭＲ及元素分析鉴定．使用氧指数，塑化效率、拉伸伸长率及差热分析研究其阻燃、增塑性能及热稳定性。
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| 关 键 词： | 四溴邻苯二甲酸双酯，相转移催化，阻燃剂，增塑，热稳定性 |
A Study on Solid-Liquid Phase Transfer Catalytic Synthesis of Tetrabromophthalate Dialkyl Esters |
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| Wang Xiaomei, Wang Xikui, Xu Guangtong, Mong Pingrui.A Study on Solid-Liquid Phase Transfer Catalytic Synthesis of Tetrabromophthalate Dialkyl Esters[J].Chinese Journal of Applied Chemistry,1995(4). |
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| Authors: | Wang Xiaomei Wang Xikui Xu Guangtong Mong Pingrui |
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| Abstract: | Eighteen title compounds were synthesized by phase transfer catalysis.The aver-age yields are over 90%. For the obtained flame retardants,their structures were identifiedby IR,NMR and elemental analysis,and their properties of the flame retardation and plasti-cization have also been investigated. |
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| Keywords: | tetrabromophthalate dialkyl ester phase transfer catalysis flame retardant plas-ticization thermostability |
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