Chemoselective Protection of Hydroxyl Groups and Deprotection of Silyl Ethers |
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| Authors: | Babasaheb P Bandgar Suhas P Kasture |
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| Institution: | (1) Organic Chemistry Research Laboratory, School of Chemical Sciences, Swami Ramanand Teerth Marathwada University, Nanded-431606, India, IN |
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| Abstract: | Summary. Trimethylsilylation of alcohols and phenols is carried out using hexamethyldisilazane and LiClO4 under microwave irradiation and neutral conditions. The deprotection of silyl ethers is carried out similarly using natural
kaolinitic clay and a few drops of water.
Received March 1, 2001. Accepted (revised) April 17, 2001 |
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| Keywords: | , ,Silyl ethers, Alcohols, Phenols, Protection, Deprotection, |
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