Direct detection of nitrogen-14 in solid-state NMR spectroscopy |
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| Authors: | O'Dell Luke A |
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| Affiliation: | Steacie Institute for Molecular Sciences, National Research Council, 100 Sussex Drive, Ottawa, Ontario, Canada K1N 5A2 |
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| Abstract: | |
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| Keywords: | Abbreviations: A-β, amyloid-β ADRF, adiabatic demagnetization in the rotating frame C16TAB, n-hexadecyltrimethylammonium bromide CP, cross polarization CS, chemical shift CSA, chemical shift anisotropy CW, continuous wave DANTE, delays alternating with nutation for tailored excitation DAPT, dipolar assisted polarization transfer DAS, dynamic angle spinning DDAB, didodecyldimethylammonium bromide DEISM, direct enhancement of integer spin magnetization DFT, density functional theory DIPOTSHIFT, dipolar overtone shift DISQUO, dipolar splittings, quadrupolar offset DMPC, dimyristoyl phosphatidylcholine DPPC, dipalmitoyl phosphatidylcholine EFG, electric field gradient EPC, egg yolk phosphatidylcholine EXPRESS, exchange program for relaxing spin systems FID, free induction decay FOQI, first-order quadrupolar interaction HMT, hexamethylenetetramine LC, liquid crystal MAS, magic angle spinning NAV, N-acetylvaline ORR, overtone rotary recoupling PISEMA, polarization inversion spin exchange at magic angle QCPMG, quadrupolar Carr Purcell Meiboom Gill RF, radio frequency RotIsseRIe, reorientation-induced redistribution of isochromats S/N, signal to noise ratio SLF, separated local field SOQI, second-order quadrupolar interaction STARS, spectrum analysis for rotating solids STEAMER, slow turning for echo amplitude modulation and echo reduction WURST, wideband, uniform rate, smooth truncation XRD, X-ray diffraction |
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