Synthesis and Characterization of Nanocrystalline Zinc Aluminum Spinel by a New Sol-Gel Method期刊界 All Journals 搜尽天下杂志传播学术成果专业期刊搜索期刊信息化学术搜索

Synthesis and Characterization of Nanocrystalline Zinc Aluminum Spinel by a New Sol-Gel Method

Authors:	Xiulan?Duan author-information" > author-information__contact u-icon-before" > mailto:xlduan@icm.sdu.edu.cn" title=" xlduan@icm.sdu.edu.cn" itemprop=" email" data-track=" click" data-track-action=" Email author" data-track-label=" " >Email author,Duorong?Yuan,Xinqiang?Wang,Hongyan?Xu

Affiliation:	(1) State Key Laboratory of Crystal Materials, Shandong University, Jinan, 250100, People’s Republic of China

Abstract:	Using Al(OⁱPr)₃ (aluminium-iso-propoxide) and Zn(NO₃)₂⋅ 6H₂O as starting materials, HNO₃ as catalyst, ZnAl₂O₄ spinel nanometer powders were prepared at lower sintering temperatures. The gels and sintered samples of ZnAl₂O₄ were characterized by means of thermogravimetry and differential scanning calorimetry (TG/DSC), X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectra and transmission electron microscope (TEM). Pure ZnAl₂O₄ spinel nanometer powders were produced by calcining the gel above 450^∘C, with the crystallite size of 7–20 nm in the temperature range of 500–900^∘C.

Keywords:	nanomaterial sol-gel X-ray diffraction
本文献已被 SpringerLink 等数据库收录！