| 毛细管气相色谱法测定12种农药的有效成分 |
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| 引用本文： | 黄惠玲,张薇君. 毛细管气相色谱法测定12种农药的有效成分[J]. 色谱, 2001, 19(4): 347-349 |
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| 作者姓名： | 黄惠玲 张薇君 |
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| 作者单位： | 海南出入境检验检疫局, |
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| 摘 要： | 建立了毛细管气相色谱法测定速克灵、戊唑醇等 12种农药中有效成分的方法。采用SE 3 0大口径毛细管柱和火焰离子化检测器 (FID) ,内标法定量 ,气相色谱 /质谱法定性确证 ,样品加标的平均回收率为 99 2 0 %～10 2 4 4 % ,相对标准偏差为 0 0 7%～ 5 4 9%。该方法简单快速 ,结果准确 ,可作为测定单样、复配样农药或同时测定多种农药有效成分的通用方法
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| 关 键 词： | 毛细管气相色谱法 农药 有效成分 |
| 文章编号： | 1000-8713(2001)04-0347-03 |
| 修稿时间： | 2000-10-30 |
Determination of Active Ingredients of12 Pesticides by Capillary Gas Chromatography |
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| HUANG Hui ling,ZHANG Wei jun. Determination of Active Ingredients of12 Pesticides by Capillary Gas Chromatography[J]. Chinese journal of chromatography, 2001, 19(4): 347-349 |
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| Authors: | HUANG Hui ling ZHANG Wei jun |
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| Affiliation: | Hainan Entry-Exit Inspection and Quarantine Bureau, Haikou 570105, China. |
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| Abstract: | A method for the determination of the active ingredients of 12 pesticides, including procymidone and tebuconazole, with capillary gas chromatography has been developed A wide bore capillary column(SE 30) and FID detector were employed The internal standards were used for quantitative determination and GC/MS for qualitative determination The average recoveries were 99 20% 102 44% while the relative standard deviations were within the range of 0 07% to 5 49% The method is simple, practical and accurate for the determination of the active ingredients of individual pesticide, formulation or multi pesticides as a whole |
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| Keywords: | capillary gas chromatography pesticide active ingredient |
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