Copper p-toluenesulfonate/acetic acid: a recyclable synergistic catalytic system for the tetrahydropyranylation of alcohols and phenols |
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Authors: | Min Wang Zhi-Guo Song Heng Jiang Hong Gong |
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Affiliation: | (1) College of Chemistry and Chemical Engineering, Bohai University, Jinzhou, China;(2) Center for Science and Technology Experiment, Bohai University, Jinzhou, China;(3) Liaoning Shihua University, Fushun, China |
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Abstract: | Copper p-toluenesulfonate/acetic acid was found to be an efficient, chemoselective synergistic catalytic system, with catalyst loading as low as 0.3 mol% leading to clean, high-yielding tetrahydropyranylation of a variety of alcohols and phenols. By simple phase-separation, copper p-toluenesulfonate can be easily recovered and reused for several times without deterioration in catalytic activity. Correspondence: Min Wang, College of Chemistry and Chemical Engineering, Bohai University, Jinzhou, China. |
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Keywords: | Tetrahydropyranylation Alcohols and phenols Synergistic catalysis Chemoselectivity Reusability. |
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