| 色谱／质谱定量分析技术在纺织品禁用偶氮染料测试中的应用 |
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| 引用本文： | 陈军.色谱／质谱定量分析技术在纺织品禁用偶氮染料测试中的应用[J].分析化学,1998,26(5):501-505. |
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| 作者姓名： | 陈军 |
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| 作者单位： | 苏州进出口商品检验局!苏州215004(陈军)，上海同济大学污染控制实验室!上海200092(陈正夫) |
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| 摘 要： | 建立了偶氮染料印染的纺织品中有害芳胺的ＧＣ／ＭＳ定量分析方法。
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| 关 键 词： | 织物 偶氮染料 芳香胺 禁用 芳胺 分析 色质联用 |
Application of Gas Chromatography /Mass Spectrometry Quantitative Identification for Prohibited Azo -Dyes on Textiles |
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| Chen Jun..Application of Gas Chromatography /Mass Spectrometry Quantitative Identification for Prohibited Azo -Dyes on Textiles[J].Chinese Journal of Analytical Chemistry,1998,26(5):501-505. |
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| Authors: | Chen Jun |
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| Abstract: | The development of a GC/MS quantitive analysis method has been described for the determination of hazardous arylamines on the textiles dyed with the azo-dyes. Azodyestuff on the textile samples can be converted into the initial intermate amines while being processed by sodium dithionite reductive system in the buffer media (pH=6), After an offline solid-phase extraction and clean-up procedure, extraction solution can be detected and confirmed by gas chromatograhy with mass selective detection. The detection limits for the arylamines are in the range of 15-30 mg/kg samples. The average recovery is 83%. The representative textile samples have been undertaken by this quantiative analysis and comparity test successfully. |
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| Keywords: | Textiles azo-dyes arylamine gas chromatography/mass spectrometry |
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