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核桃仁中多酚类物质的液相/电喷雾质谱分析
引用本文:王克建,杜明,胡小松,齐建勋,郝艳宾.核桃仁中多酚类物质的液相/电喷雾质谱分析[J].分析化学,2009,37(6).
作者姓名:王克建  杜明  胡小松  齐建勋  郝艳宾
作者单位:1. 北京市农林科学院林业果树研究所,北京,100093
2. 哈尔滨工业大学食品科学与工程学院,哈尔滨,150090
3. 中国农业大学食品科学与营养工程学院,北京,100083
摘    要:利用HPLC-ESI-MSn方法对核桃(Juglans regia L.)仁中多酚类物质组成进行了分析,发现的多酚类物质有鞣花酰基葡萄糖4种异构体、橡椀酰基葡萄糖2种异构体、二鞣花酰基葡萄糖2种异构体、二没食子酰基葡萄糖2种异构体、鞣花酰基和橡椀酰基葡萄糖3种异构体.结果表明,采用HPLC-ESI-MSn方法可以对核桃仁中多酚类物质进行有效的分析.

关 键 词:核桃仁  没食子单宁  鞣花单宁  液相色谱/电喷雾质谱

Identification of Phenolic Compounds in Walnut (Juglans regia L) Seeds by High Performance Liquid Chromatography Electrospray Ionization Mass Spectrometry
WANG Ke-Jian,DU Ming,HU Xiao-Song,QI Jian-Xun,HAO Yan-Bin.Identification of Phenolic Compounds in Walnut (Juglans regia L) Seeds by High Performance Liquid Chromatography Electrospray Ionization Mass Spectrometry[J].Chinese Journal of Analytical Chemistry,2009,37(6).
Authors:WANG Ke-Jian  DU Ming  HU Xiao-Song  QI Jian-Xun  HAO Yan-Bin
Institution:Institute of Forestry & Pomology;Beijing Academy of Agriculture and Forestry Sciences;Beijing 100093;College of Food Science and Engineering;Harbin Institute of Technology;Harbin 150090;College of Food Science & Nutritional Engineering;China Agricultural University;Beijing 100083
Abstract:High performance liquid chromatography coupled with electrospray ionization mass spectrometry was used to study the phenolics profile of Persian walnut(Juglans regia L.) seeds.Four isomers of HHDP(Hexahydroxydiphenoyl)-glucopyranose,2 isomers of valoneoyl-glucopyranose,2 isomers of di-HHDP-glucopyranose,3 isomers of galloy-valoneoyl-glucopyranose and 2 isomers of digalloy-glucopyranose were found to be present in Persian walnut seeds with a number of,as yet,unknown compounds.The results illustrate that the ...
Keywords:Walnut seeds  gallotannins  ellagitannins  high performance liquid chromatography coupled with electrospray ionization mass spectrometry  
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