| 研磨法合成N-芳亚甲基-4-氨基安替比林 |
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| 引用本文： | 胡蔚昱,李毅群,张莉萍. 研磨法合成N-芳亚甲基-4-氨基安替比林[J]. 合成化学, 2007, 15(4): 475-476 |
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| 作者姓名： | 胡蔚昱 李毅群 张莉萍 |
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| 作者单位： | 怀化学院,化学化工系,湖南,怀化,418000;暨南大学,化学系,广东,广州,510632 |
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| 摘 要： | 在室温和无溶剂研磨条件下,氯化锌催化一系列芳醛与4-氨基安替比林反应生成相应的席夫碱,收率81%~91%。
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| 关 键 词： | 氯化锌 氨基安替比林 芳醛 席夫碱 固相反应 |
| 文章编号： | 1005-1511（2007）04-0475-02 |
| 收稿时间： | 2006-05-16 |
| 修稿时间： | 2006-05-16 |
Synthesis of N-arylidene-4-aminoantipyrine by Grinding Method |
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| HU Wei-yu,LI Yi-qun,ZHANG Li-ping. Synthesis of N-arylidene-4-aminoantipyrine by Grinding Method[J]. Chinese Journal of Synthetic Chemistry, 2007, 15(4): 475-476 |
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| Authors: | HU Wei-yu LI Yi-qun ZHANG Li-ping |
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| Affiliation: | 1. Department of Chemistry, Jinan University, Guangzhou 510632, China; 2. Department of Chemistry and Chemical Engineering, Huaihua College, Huaihua 418000, China |
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| Abstract: | The rapidly condensation of 4-aminoantipyrine and aryl aldehydes was efficiently catalyzed by zinc chloride to corresponding Schiff bases at room temperature in 81%~91% yields under solvent-free conditions by grinding method. |
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| Keywords: | zinc chloride aminoantipyrine aromatic aldehyde Schiff base solide reaction |
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