Synthesis and Crystal Structure of Tetrabutylammonium 4-(2-Bromothiophene-5-Sulfanilamide)-Benzoate |
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| Authors: | Jing Xiong Yun Guo Zhen-Yu Li Zhi Min Jin |
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| Institution: | (1) College of Chemistry and Materials Engineering, Wenzhou University, Wenzhou, 325027, People’s Republic of China;(2) College of Pharmaceutical Sciences, Zhejiang University of Technology, Hangzhou, 310014, People’s Republic of China;(3) Zhejiang Environmental Monitoring Centre, Hangzhou, 310012, People’s Republic of China; |
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| Abstract: | Abstract Tetrabutylammonium 4-(2-bromothiophene-5-sulfanilamide)-benzoate crystallizes in C2/C lattice with a = 18.3389(17), b = 16.540(16), c = 15.8280(15) ?, β = 116.959(2), V = 4279.5(7) ?3, Z = 4, and R = 0.0560. In the structure a very short centrosymmetric hydrogen bond and C=O···Br halogen bond interactions, together with
N–H···O and C–H···O hydrogen bonds give a three-dimensional network. |
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