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制备工艺对B4C/TiB2/Mo/C陶瓷复合材料力学性能和显微结构的影响
引用本文:孙军龙,邓建新,刘长霞.制备工艺对B4C/TiB2/Mo/C陶瓷复合材料力学性能和显微结构的影响[J].人工晶体学报,2006,35(4):844-848,834.
作者姓名:孙军龙  邓建新  刘长霞
作者单位:山东大学机械工程学院,济南,250061
基金项目:ProjectsupportedbytheNaturalScienceFoundationofShandongProvince(Y2004F08),theSpecializedResearchFundfortheDoctoralProgramofHigherEducation(20030422105)andtheSustainProjectofNewCenturyExcellenceTalent(NCET-04-0622)
摘    要:采用热压法制备了80.6?C/11.6%TiB2/4.7%Mo/3%C质量分数陶瓷复合材料,分析了烧结工艺对力学性能和微观结构的影响。烧结温度变化范围是1800~1950℃,保温时间变化范围是15~60m in,烧结压力30~35MPa。当烧结参数为1900℃、45m in、35MPa,B4C/TiB2/Mo/C陶瓷复合材料抗弯强度、硬度、韧性、相对密度分别为705MPa、20.6GPa、3.82MPa.m1/2、98.2%。

关 键 词:B_4C  烧结  力学性能  微结构
文章编号:1000-985X(2006)04-0844-05
收稿时间:2005-12-22
修稿时间:2005-12-22

Influence of Sintering Technique on Mechanical Properties and Microstructure of B4C/TiB2/Mo/C Composite
SUN Jun-long,DENG Jian-xin,LIU Chang-xia.Influence of Sintering Technique on Mechanical Properties and Microstructure of B4C/TiB2/Mo/C Composite[J].Journal of Synthetic Crystals,2006,35(4):844-848,834.
Authors:SUN Jun-long  DENG Jian-xin  LIU Chang-xia
Abstract:80.6wt.%B4C/11.6wt.%TiB2/4.7wt%Mo/3wt.%C ceramic composite is fabricated by hot-pressing sintering and the effect of sintering temperature, holding time and pressure on mechanical properties and microstructure of the composite are analyzed. The temperature is raised from 1800℃ to 1950℃, the holding time ranges from 15min to 60min and the pressure is 30-35MPa. The strength, hardness, toughness and densification of the composite prepared by the optimized process of 1900℃ under 35MPa for 45min are 705MPa, 20.6GPa, 3.82MPa·m1/2, 98.2%, respectively.
Keywords:B_4C  sintering technique  mechanical properties  microstructure
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