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火焰原子吸收光谱法直接测定金锭中银、铜、铁、铅、锑和秘的含量
引用本文:倪迎瑞,李中玺,李海涛.火焰原子吸收光谱法直接测定金锭中银、铜、铁、铅、锑和秘的含量[J].广东微量元素科学,2011,18(11):49-52.
作者姓名:倪迎瑞  李中玺  李海涛
作者单位:陕西黄金集团西安秦金有限责任公司,陕西 西安710054;西北有色地质研究院,陕西 西安710054
基金项目:国家中小企业创新基金项目资助
摘    要:通过火焰原子吸收光谱法直接测定了金锭中Ag、Cu、Fe、Pb、Bi、Sb的含量.结果表明,该法可极大地缩短分析时间,方法的检出限Ag、Cu、Fe、Pb、Bi、Sb分别为0.008、0.020、0.015、0.032、0.22、0.25 μg/mL;回收率94%~108%;RSD小于1.8%.该法快速、简便、准确.

关 键 词:金锭  火焰原子吸收光谱法      

Determination of Ag, Cu, Fe, Pb, Sb and Bi in Gold Ingot by FAAS
NI Yingrui,LI Zhongxi,LI Haitao.Determination of Ag, Cu, Fe, Pb, Sb and Bi in Gold Ingot by FAAS[J].Trace Elements Science,2011,18(11):49-52.
Authors:NI Yingrui  LI Zhongxi  LI Haitao
Institution:1. Xi'an Qinjing Limited Liability Company of Shannxi Gold, Xi'an 710054, China; 2. Northwest Nonferrous Geological Research Institute, Xi'an 710054, China; )
Abstract:The simultaneous determination of Ag, Cu, Fe, Pb, Bi and Sb in gold ingot by flame atomic absorption spectrometry(FAAS) was proposed. The detection limits for Ag, Cu, Fe, Pb, Bi and Sb were 0. 008, 0. 020, 0. 015, 0. 032, 0. 22 and 0. 25 μg/mL. The recoveries for six elements were between 94% - 108% and the relative standard deviations were less than 1.8% , the method is rapid, and convenient accurate.
Keywords:gold ingot  FAAS  Ag  Cu  Fe
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