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| 签字笔墨迹的光老化及书写时间变化规律的研究 | |
| 引用本文： | 赵鹏程,王彦吉,徐媛媛,王景翰.签字笔墨迹的光老化及书写时间变化规律的研究[J].光谱学与光谱分析,2008,28(10):2348-2351. |
| 作者姓名： | 赵鹏程 王彦吉 徐媛媛 王景翰 |
| 作者单位： | 1. 中国刑事警察学院法化系，辽宁 沈阳 110035 2. 中国人民公安大学，北京 100038 3. 东北师范大学化学系，吉林 长春 130024 |
| 基金项目： | 国家高技术产业发展项目，国家"十一五"科技支撑计划项目资助 |
| 摘 要： | 利用日光和紫外光对黑色签字笔字迹样本进行了光老化处理，通过区带毛细管电泳法分析了签字笔字迹墨水提取液，二极管阵列检测器记录了190～600 nm波长范围内的物质吸收峰，用电泳图中不同波长不同迁移时间的电泳峰面积之比对老化时间作图，得出了墨水中不同染料间含量的相对变化关系相对于老化时间的变化规律。同时也对自然老化的签字笔样品随书写时间的变化规律进行了研究。 |
| 关 键 词： | 签字笔墨水 毛细管电泳 光老化 书写时间 |
| 收稿时间： | 2008-01-08 |
Investigation of Accelerated Aging in Light and Writing Age of Roller Pen Inks |
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| ZHAO Peng-cheng,WANG Yan-ji,XU Yuan-yuan,WAN Jing-han.Investigation of Accelerated Aging in Light and Writing Age of Roller Pen Inks[J].Spectroscopy and Spectral Analysis,2008,28(10):2348-2351. | |
| Authors: | ZHAO Peng-cheng WANG Yan-ji XU Yuan-yuan WAN Jing-han |
| Institution: | 1. Forensic Chemistry Department of China Criminal Police College, Shenyang 110035，China2. Chinese People Public Security University, Beijing 100038，China3. Chemistry Department of North East Normal University, Changchun 130024，China |
| Abstract: | The aging of roller pen ink entries was accelerated in sunlight and ultraviolet, and the extracts of roller pen inks on paper were analyzed by capillary zone electrophoresis, photo diode array (PDA) detector. Scanning range of 190-600 nm was adopted in experiment and the change curves were obtained by the plot of the ratio of peak areas in electrophoretogram vs. accelerated aging. The rule of accelerated aging of roller pen ink was investigated by relative changes in content between different dyes in inks. In addition, the relative writing age of roller pen entries was investigated. |
| Keywords: | Roller pen inks Capillary electrophoresis Aging in light Writing age |
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