| 苦黄注射液中大黄蒽醌含量测定方法改进 |
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| 引用本文： | 宗水珍,汪学英.苦黄注射液中大黄蒽醌含量测定方法改进[J].分析测试学报,2000,19(6):59-60. |
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| 作者姓名： | 宗水珍 汪学英 |
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| 作者单位： | 常熟高等专科学校生化系,江苏,常熟,215500 |
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| 摘 要： | 按苦黄注射液原质量标准（草案）中测定方法,大黄蒽醌用氯仿提取,阴性试验结果为苦黄注射液大黄蒽酯标示量的１６．５０％（ｎ＝５）,结果偏高;改用石油醚提取,降为６．１５％,重复性试验的ＲＳＤ为１．４４％（ｎ＝５）,加标回收率为１０１．８％（ｎ＝５）,显色在１－４ｈ内稳定,表明该法是可行的。
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| 关 键 词： | 苦黄注射液 大黄蒽酯 阴性试验 中药分析 光度法 |
Improvement of Method for Determination of Content of Anthraquinone from Radix et Rhizoma Rhei in Kuhuang Injection |
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| ZONG Shui-zhen,WANG Xue-ying.Improvement of Method for Determination of Content of Anthraquinone from Radix et Rhizoma Rhei in Kuhuang Injection[J].Journal of Instrumental Analysis,2000,19(6):59-60. |
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| Authors: | ZONG Shui-zhen WANG Xue-ying |
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| Abstract: | Anthraquinone from Radix et Rhizoma Rhei is extracted by chloroform in accordance with the method of the quality standard(draft) of Kuhuang injection. The result of negative test is 16.50% of the nominal value of anthraquinone from Radix et Rhizoma Rhei in Kuhuang injection, which is unacceptably high. An improved method for the determination is proposed by using petroleum ether as an extractant instead of chloroform. By using the proposed method the determination result of negative test for the an- thraquinone is lowered to 6.15%. The RSD and recovery of the method is 1.44% and 101. 8%, re- spectively, furthermore coloration is stable. Therefore, it is feasible. |
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| Keywords: | Kuhuang injection Radix et Rhizoma Rhei Anthraquinone Negative test |
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