The synthesis of (4S,5S)-(?)-isocytoxazone |
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Authors: | Maria D Rozwadowska Anna Tomczak |
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Institution: | Faculty of Chemistry, A. Mickiewicz University, ul. Grunwaldzka 6, 60-780 Poznań, Poland |
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Abstract: | (4S,5S)-(?)-Isocytoxazone, which is needed for a configurational study, was synthesized from the commercially available (1S,2S)-(+)-2-amino-1-(4-nitrophenyl)-1,3-propanediol in which the p-nitro substituent was replaced by a p-methoxyl group; the thus prepared p-methoxyphenyl amino diol was cyclized via an N-Boc derivative. |
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