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Crystal growth,structural and photoluminescence studies of L-tyrosine hydrobromide semi organic single crystal
Authors:P. Anandan  S. Vetrivel  R. Jayavel  C. Vedhi  G. Ravi  G. Bhagavannarayana
Affiliation:1. Centre for Materials Research, Thiruvalluvar College of Engineering and Technology, Ponnur Hills, Vandavasi 604 505, India;2. Post Graduate and Research Department of Physics, Government Arts College, Thiruvannamalai 606 603, India;3. Crystal Growth Centre, Anna University, Chennai 600 025, India;4. Department of Chemistry, V.O. Chidhambaram College, Tuticorin 628 008, India;5. Department of Physics, Alagappa University, Karaikudi 630 003, India;6. Materials Science Division, National Physical Laboratory, Dr. K.S. Krishnan Road, New Delhi 110 012, India
Abstract:Nearly perfect single crystal of L-tyrosine hydrobromide (LTHB) has been grown at room temperature from the saturated solution prepared from the solvent with optimised normality (2N) using slow evaporation solution growth technique. Crystal system and lattice parameters have been estimated by single crystal X-ray diffraction analysis. Prominent peeks of powder X-ray diffraction pattern have been indexed and diffraction data have been presented. The presence of various functional groups in LTHB has been identified by vibrational and Nuclear Magnetic Resonance spectral study. The crystalline nature and defect during the growth has been studied by obtaining high resolution X-ray diffraction curve (rocking curve) for the title crystal and detailed explanation is given in this paper. Cyclic voltammetric behaviour and photoluminescence properties of LTHB have also been investigated.
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