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| 陈皮挥发油的气相色谱/质谱分析 | |
| 引用本文： | 龚范,梁逸曾,宋又群,彭源贵,崔卉,Chau Foo-tim. 陈皮挥发油的气相色谱/质谱分析[J]. 分析化学, 2000, 28(7): 860-864 |
| 作者姓名： | 龚范 梁逸曾 宋又群 彭源贵 崔卉 Chau Foo-tim |
| 作者单位： | 1. 湖南大学化学化工学院化学计量学与化学传感技术研究所,长沙,410082 2. 湖南省中医药研究院中药研究所,长沙,410013 3. 香港理工大学应用生物化学技术系,香港九龙 |
| 基金项目： | 国家自然科学基金!（29875007） |
| 摘 要： | 用ＧＣ／ＭＳ分析复方制剂平胃散中的一种单味药材陈皮的挥发油化学成分及其相对含量，对色质联用仪产生的二维数据借助直观推导式演进特征投影法来分辨以得到组分的纯色谱和质谱，根据组分的色谱保留时间和质谱对组分进行定性，继而用总体积积分法定量。本文分离出５３个组分，其中鉴定了３４个组分，约占其挥发油总量的９６．０８％。 |
| 关 键 词： | 气相色谱／质谱 陈皮 挥发油 中药 化学成分分析 |
Determination of the Volatile Oil of Pericarpium Citri Reticulatae with Gas Chromatography/Mass Spectrometry |
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| Cong Fan,Liang Yizeng,Song Youqun,Peng Yungui,Cui Hui,Leung Alexander Kai-man,Chau Foo-tim. Determination of the Volatile Oil of Pericarpium Citri Reticulatae with Gas Chromatography/Mass Spectrometry[J]. Chinese Journal of Analytical Chemistry, 2000, 28(7): 860-864 | |
| Authors: | Cong Fan Liang Yizeng Song Youqun Peng Yungui Cui Hui Leung Alexander Kai-man Chau Foo-tim |
| Affiliation: | Cong Fan,Liang Yizeng,Song Youqun(College of Chemistry and Chemical Engineering,Institute of Chemometrics and Chemiclal Sensing Technology,,Hu' nan Uniuersity Changsha 410082)Peng Yungui(Institute of Materia Medica,Hu' nan Academy of Traditional Chinese Medicine & Materia Medica,Changsha 410013)Cui Hui(College of Chemistry and Chemical Engineering,Institute of Chemometrics and Chemiclal Sensing Technology,,Hu' nan Uniuersity Changsha 410082)Leung Alexander Kai-man(Departmemt of Applied Biology and Chemical Technology,The Hongkong Polytechnic Uniuersity,Kowloon,Hongkong) |
| Abstract: | A method for determining chemical components of the volatile oil of Pericarpium Citri Reticulatae with gas chromatography/mass spectrometry was investigated. With the help of heuristic evolving latent projections (HELP) resolution and overall volume integration method upon two-way data, 53 components were separated and 34 of them were qualitatively and quantitatively analyzed representing about 96. 08 % of the total content. |
| Keywords: | Gas chromatography/mass spectrometry heuristic evolving latent Projections Pericarpium Citri Reticulatae volatile oil |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |