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4,5-, 3,6-, and 3,4,5,6-tert-Butylsulfanylphthalonitriles: synthesis and comparative structural and spectroscopic analyses
Authors:Ufuk Kumru  Fabienne Dumoulin  Erwann Jeanneau  Fatma Yuksel  Yari Cabezas  Yunus Zorlu  Vefa Ahsen
Institution:1. Department of Chemistry, Gebze Institute of Technology, P. O. Box 141, 41400, Gebze, Kocaeli, Turkey
2. CNRS UMR 5615, Laboratoire des Multimatériaux et Interfaces, Université Lyon1, 69622, Villeurbanne, France
3. Ecole Nationale Supérieure de Chimie de Clermont-Ferrand, Clermont Université, BP 10448, 63000, Clermont-Ferrand, France
Abstract:Three tert-butylsulfanylphthalonitriles have been prepared with optimized synthetic procedures. Their comparative structural analyses have been completed, with a focus on IR and NMR spectroscopy and refined X-ray structural data. Miscellaneous parameters such as UV absorption, melting points, and related polarity of the compounds are summarized.
Keywords:
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