| 钯催化氧化/水解2-炔基芳基叠氮一锅法合成2-苯甲酰胺基苯甲酸 |
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| 引用本文： | 圣戎,李萍,周志强,胡贵文,张小祥. 钯催化氧化/水解2-炔基芳基叠氮一锅法合成2-苯甲酰胺基苯甲酸[J]. 有机化学, 2020, 0(2): 462-469 |
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| 作者姓名： | 圣戎 李萍 周志强 胡贵文 张小祥 |
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| 作者单位： | 南京林业大学化工学院江苏省生物质绿色燃料与化学品重点实验室 |
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| 基金项目： | 江苏省研究生创新计划(No.KYCX18_0967);国家自然科学基金(No.21302096);江苏省自然科学基金(No.BK20171449);江苏高校“青蓝工程”资助项目. |
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| 摘 要： | 描述了通过钯催化2-炔基芳基叠氮一锅法氧化/水解制备2-苯甲酰胺基苯甲酸的合成方法.在温和的反应条件下,反应以良好至极好的产率完成.
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| 关 键 词： | 钯催化 一锅化反应 氧化 水解 2-苯甲酰氨基苯甲酸 |
Pd-Catalyzed One-Pot Oxidation/Hydrolysis for the Synthesis of 2-Benzoylaminobenzoic Acids from 2-Alkynyl Arylazides |
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| Sheng Rong,Li Ping,Zhou Zhiqiang,Hu Guiwen,Zhang Xiaoxiang. Pd-Catalyzed One-Pot Oxidation/Hydrolysis for the Synthesis of 2-Benzoylaminobenzoic Acids from 2-Alkynyl Arylazides[J]. Chinese Journal of Organic Chemistry, 2020, 0(2): 462-469 |
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| Authors: | Sheng Rong Li Ping Zhou Zhiqiang Hu Guiwen Zhang Xiaoxiang |
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| Affiliation: | (College of Chemical Engineering,Jiangsu Key Laboratory of Biomass-based Green Fuels and Chemicals,Nanjing Forestry University,Nanjing 210037) |
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| Abstract: | A synthetic method to prepare 2-benzoylaminobenzoic acids via Pd-catalyzed one-pot oxidation/hydrolysis from 2-alkynyl arylazides is described. The reaction was accomplished in good to excellent yields under mild reaction conditions. |
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| Keywords: | Pd-catalyzed one-pot reaction oxidation hydrolysis 2-benzoylaminobenzoic acids |
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