| 2-(1H-1,2,4-三唑-1-基)-4,4-二甲基-1-烃硫基-3-戊酮的合成及波谱性质 |
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| 引用本文： | 张耀谋,金桂玉.2-(1H-1,2,4-三唑-1-基)-4,4-二甲基-1-烃硫基-3-戊酮的合成及波谱性质[J].广州化学,2000,25(3):22-25. |
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| 作者姓名： | 张耀谋 金桂玉 |
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| 作者单位： | 1. 中国科学院广州化学研究所,广州,510650
2. 南开大学元素有机化学研究所,元素有机化学国家重点实验室,天津,300071 |
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| 基金项目： | 广东省博士启动基金，， |
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| 摘 要： | 由 2 - (1H - 1 ,2 ,4-三唑 - 1 -基 ) - 4 ,4-二甲基 - 1 -戊烯 - 3 -酮和硫酚 (醇 )亲核加成反应合成了五个未见文献报道的目标化合物 ,其化学结构经IR、1 HNMR、MS和元素分析确证并研究其波谱性质
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| 关 键 词： | 1 4-亲核加成 1 2 4-三唑 波谱性质 |
| 修稿时间： | 2000-03-28 |
Synthesis and Spectrum Properties of 1-Alkylthio-2-(1H-1,2,4-Triazole-1-yl)-4,4-Dimethyl-3-Pentone |
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| Zhang Yaomou,Jin Guiyu.Synthesis and Spectrum Properties of 1-Alkylthio-2-(1H-1,2,4-Triazole-1-yl)-4,4-Dimethyl-3-Pentone[J].Guangzhou Chemistry,2000,25(3):22-25. |
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| Authors: | Zhang Yaomou Jin Guiyu |
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| Abstract: | Five title compounds were synthesized through the additional reaction of 2-(1H-1,2,4-triazolyl-1-yl)-4,4-dimethyl-1-pentene-3-one with arylthiol, which were identified by IR、 1H NMR、MS and elemental analysis. Spectrum properties of title compounds were also studied. |
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| Keywords: | additional reaction 1 2 4-triazole spectrum properties |
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