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Microwave-assisted fast and efficient synthesis of some crown ethers
Authors:Ahmad Ziafati  Hossein Eshghi  Omolbanin Sabzevari
Affiliation:Department of Chemistry, Ferdowsi University of Mashhad, P.O. Box 91775-1436, Mashhad, Iran
Abstract:13-Crown-4,16-crown-5,dibenzo-12-crown-4 and dibenzo-14-crown-4 were synthesized by a one-pot microwave-assisted procedure in good yields.Irradiation of diols and dichlorides in the presence of sodium hydroxide in DMSO gave title crown ethers presumably within a template effect.
Keywords:Crown ether  Microwave irradiation  Template effect
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