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| 尖晶石型纳米铁酸镍的制备与磁性研究 | |
| 引用本文： | 莎木嘎,娜仁图雅,莫日根图,李金梅,赵智宏.尖晶石型纳米铁酸镍的制备与磁性研究[J].光谱实验室,2009,26(4):876-880. |
| 作者姓名： | 莎木嘎 娜仁图雅 莫日根图 李金梅 赵智宏 |
| 作者单位： | 1. 内蒙古农业大学理学院无机及分析化学教研室,呼和浩特市昭乌达路306号,010018 2. 呼和浩特民族学院,呼和浩特市通道北路56号,010051 3. 水利部牧区水利科学研究所内蒙古,呼和浩特市大学东路16号,010010 |
| 基金项目： | 内蒙古自治区高等学校科学研究项目 |
| 摘 要： | 以Fe（NO3）3·9H2O和Ni（NO3）2·6H2O为原料,用柠檬酸为还原剂,采用燃烧法制备了NiFe2O4纳米粉体,用X射线粉末衍射仪（XRD）、透射电子显微镜（TEM）、红外光谱（IR）和振动样品磁强计（VSM）等手段对样品进行了表征,结果表明,样品为立方晶系尖晶石铁酸镍纳米粉体,其粒径在20—40nm之间,具有超顺磁性,并探讨了焙烧温度、焙烧时间对样品磁性的影响。 |
| 关 键 词： | 纳米粉体 燃烧法 尖晶石型 立方晶系 超顺磁性 |
Preparation of Spinel-Type Nano-Sized NiFe2O4 Powder and Magnetic Study |
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| SHA Mu-Ga,NA Ren-Tuya,MO Ri-Gentu,LI Jin-Mei,ZHAO Zhi-Hong.Preparation of Spinel-Type Nano-Sized NiFe2O4 Powder and Magnetic Study[J].Chinese Journal of Spectroscopy Laboratory,2009,26(4):876-880. | |
| Authors: | SHA Mu-Ga NA Ren-Tuya MO Ri-Gentu LI Jin-Mei ZHAO Zhi-Hong |
| Institution: | SHA Mu-Ga, NA Ren-Tuya, MO Ri-Gentu, LI Jin-Mei, ZHAO Zhi-Hong (1. The Science College of Innermongolia Agricultural University, Huhehaote 010018, P. R. China; 2. Huheaohte University for Nationalities. Huhehaote 020051, P. R. China; 3.Institute of Water Resources and Hydropower Research for Pastoral Areas, Huhehaote 010010, P. R. China) |
| Abstract: | NiFe2O4 nano-powder were prepared with combusion method taking Fe（NO3）3·9H2O,Ni（（NO3）2·6H2O as raw materials and Citric Acid as reductant.The samples were tested through XRD,TEM,IR and VSM characterization. The NiFe2O4 nano-powder is cubic-crystal-system belong to spinel-model respectivesly,their particle s diameters are between 20 and 40nm with superparamagnetic property.Furthermore,the effect of roasting temperature and roasting time on the magnetism of samples were also studied. |
| Keywords: | Nano-Powder Combustion Method Spinel-Model Cubic-Crystal-System Superparamagnetic |
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