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激光诱导击穿光谱技术对火车车轮钢中成分的原位统计分布分析表征
引用本文:刘佳,沈学静,张关震,郭飞飞,李冬玲,王海舟. 激光诱导击穿光谱技术对火车车轮钢中成分的原位统计分布分析表征[J]. 光谱学与光谱分析, 2021, 41(7): 2269-2274. DOI: 10.3964/j.issn.1000-0593(2021)07-2269-06
作者姓名:刘佳  沈学静  张关震  郭飞飞  李冬玲  王海舟
作者单位:钢铁研究总院,北京 100081;钢铁研究总院,北京 100081;钢研纳克检测技术股份有限公司,北京 100081;中国铁道科学研究院集团有限公司,金属及化学研究所,北京 100081;钢研纳克检测技术股份有限公司,北京 100081
基金项目:国家重点研发计划项目(2017YFB1103900)资助
摘    要:随着铁路规模的迅速扩大,对列车运行的可靠性及耐久性的要求也越来越高,车轮作为铁路机车车辆行走系统的核心部件,它与轨道之间的摩擦既要保证安全又要提升速度,车轮材料的性能直接影响车轮对磨损和滚动接触疲劳损伤的敏感性,其服役性能也受到高度关注.研究表明,车轮钢材料的成分及分布状态可对其组织性能产生显著影响,因此,运用激光诱导...

关 键 词:激光诱导击穿光谱  原位统计分布分析  火车车轮钢  成分分布分析
收稿时间:2020-07-14

Characterization of Original Position Statistical Distribution of Composition in Train Wheel Steel by Laser-Induced Breakdown Spectrum
LIU Jia,SHEN Xue-jing,ZHANG Guan-zhen,GUO Fei-fei,LI Dong-ling,WANG Hai-zhou. Characterization of Original Position Statistical Distribution of Composition in Train Wheel Steel by Laser-Induced Breakdown Spectrum[J]. Spectroscopy and Spectral Analysis, 2021, 41(7): 2269-2274. DOI: 10.3964/j.issn.1000-0593(2021)07-2269-06
Authors:LIU Jia  SHEN Xue-jing  ZHANG Guan-zhen  GUO Fei-fei  LI Dong-ling  WANG Hai-zhou
Affiliation:1. Central Iron and Steel Research Institute, Beijing 100081, China2. NCS Testing Technology Corporation Limited, Beijing 100081, China3. Metals & Chemistry Research Institute, China of Railway Sciences Corporation Limited, Beijing 100081, China
Abstract:With the rapid expansion of the railway scale, the requirements for the reliability and durability of train operation are getting higher and higher. As the core component of the railway vehicle system, the friction between the wheel and the track must ensure safety and increase the speed. The performance of the wheel material directly affects the sensitivity of the wheel to wear and rolling contact fatigue damage, and its service performance is also highly concerned. Studies have shown that the composition and distribution of wheel steel materials can significantly impact the performance of its microstructure.Therefore, this paper aims to use the laser-induced breakdown spectroscopy technology to quickly analyze the high efficiency of multi-element, better spatial resolution, scanning analysis capabilities in a larger area and other technical advantages, combined with statistical distribution analysis method, to achieve rapid characterization of the composition and distribution of wheel steel materials. In this paper, the vertical surface of the wheel rim was selected as the analysis surface. The low time’s test showed that there were obvious thick dendrite structures in thearea away from the tread surface, and the organization structure had unevenness, and use this as a feature analysis area for sampling. 320 mesh alumina sandpaper was used for surface treatment, and the LIBSOPA system was used for component distribution analysis. First, under different ablation conditions, the spectral signal intensity and stability of each element’s characteristic spectral line were compared and analyzed, and 20 pre-ablation and 10 ablations were optimized as experimental conditions; second, using established the standard internal method to characterize the quantitative results of nine elements such as Si, Mn, P, S, Cr, Ni, Mo, Cu, V in wheel steel. The quantitative results and the results of direct-reading spectrum analysis have good consistency; In the end, the sample was scanned regionally, and the statistical distribution of each element’s composition distribution was statistically characterized. The statistical results of the composition distribution partition showed that the statistical segregation degree of all elements near the tread area was less than that away from the tread area. Based on the statistical segregation degree and the two-dimensional distribution map of the components, it can be seen that the distribution of the components of the test sample away from the tread area is uneven, and the results correspond well with the results observed by the low-times test method. In this paper, the LIBSOPA technology is used to realize the composition distribution characterization of multi-element in the train wheel steel material, which provides a new idea and characterization method for quickly determining the composition and distribution state of the wheel steel material.
Keywords:Laser-induced breakdown spectroscopy  Original position statistic distribution analysis  Wheel trerd  Components distribution analysis  
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