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DAST 源粉表征与晶体制备
引用本文:庞子博,孟大磊,窦瑛,程红娟,徐永宽.DAST 源粉表征与晶体制备[J].微波学报,2015,31(S1):105-107.
作者姓名:庞子博  孟大磊  窦瑛  程红娟  徐永宽
作者单位:( 中国电子科技集团公司第四十六研究所,天津 300220 )
摘    要:通过X 射线粉末衍射、核磁共振波谱法对制得的DAST 源粉进行表征,确证其分子结构并计算出源粉纯度为 99.7 %。然后使用该DAST 源粉配制其甲醇溶液,并利用溶液降温法通过自发成核过程培养出尺寸为(2~3) mm×(2~3) mm×(0.3~0.5) mm 的DAST 晶体。

关 键 词:太赫兹,DAST,表征,晶体

Characterization of DAST Powder and Preparation of Its Crystals
PANG Zi-bo,MENG Da-lei,DOU Ying,CHENG Hong-juan,XU Yong-kuan.Characterization of DAST Powder and Preparation of Its Crystals[J].Journal of Microwaves,2015,31(S1):105-107.
Authors:PANG Zi-bo  MENG Da-lei  DOU Ying  CHENG Hong-juan  XU Yong-kuan
Institution:(China Electronics Technology Group Corporation No. 46 Research Institute, Tianjin 300220, China)
Abstract:DAST powder prepared was characterized via X-ray powder diffraction and nuclear magnetic resonance spectrum methods. Its molecular structure was corroborated and purity of the powder calculated was 99.7 %. Then the DAST powder was used to prepare its methanol solution, and DAST crystals with size of (2~3) mm×(2~3) mm×(0.3~0.5) mm was cultivated through spontaneous nucleation process via solution temperature-reduction method.
Keywords:terahertz  DAST  characterization  crystal
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