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Structure of some products of the amidothionophosphorylation of galactitol
Authors:L. I. Gurarii  I. A. Litvinov  Yu. T. Struchkov  D. S. Yufit  B. A. Arbuzov  É. T. Mukmenev
Affiliation:(1) A. N. Nesmeyanov Institute of Heteroorganic Compounds, Academy of Sciences of the USSR, Moscow;(2) A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Branch, Academy of Sciences of the USSR, USSR
Abstract:Conclusions As a result of the successive reaction of galactitol with P(NEt2)3 and sulfur we have obtained diastereomeric galactitol 1,6-bis-O-[di(N-diethylamido)thionophosphate] 2,3:4,5-bis-O-(N-diethylamidothionophosphates) (the structure of one of them was established by x-ray diffraction analysis) and galactitol 1,2:3,4:5,6-tris-O-(N-diethylamidothionophosphates).Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 4, pp. 896–903, April, 1983.
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