| 透明莫来石陶瓷薄膜的光电子能谱研究 |
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| 引用本文： | 苏春辉,郑大方.透明莫来石陶瓷薄膜的光电子能谱研究[J].光学学报,1997,17(3):42-345. |
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| 作者姓名： | 苏春辉 郑大方 |
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| 作者单位： | [1]长春光学精密机械学院材料系 [2]吉林大学分析测试中心 |
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| 摘 要： | 采用溶胶－凝胶工艺合成了莫来石透明陶瓷薄膜。用Ｘ射线光电子能谱分析技术，通过Ｏ１ｓＡｌ２ｐ太Ｓｉ２ｐ的Ｘ射线光电子能谱分析，探讨了透明膜的结构，组成及阳离子的配位形态。研究表明，干凝胶中铝以ＡｌＯ６八面体为主，硅为ＳｉＯ４四面体，随温度的升高ＡｌＯ６向ＡｌＯ４转化，引进透明膜结构的相应变化。
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| 关 键 词： | 莫来石 透明陶瓷 薄膜 XPS |
| 收稿时间： | 1995/12/21 |
Study of Transparent Mullite Ceramic Film by XPS |
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| Su Chunhui,Wang Yan,Duanmu Qingduo.Study of Transparent Mullite Ceramic Film by XPS[J].Acta Optica Sinica,1997,17(3):42-345. |
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| Authors: | Su Chunhui Wang Yan Duanmu Qingduo |
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| Abstract: | Transparent mullite ceramic film was prepared by Sol Gel. The Structure and cation ion coordination state of transparent film were studied through analysis of O 1s 、 Al 2p and Si 2p by XPS. The study shows that aluminum is mainly octahedron of AlO 6 and silicon is tetrahedron of SiO 4 in dry gel, and AlO 6 are translated to AlO 4 with increasing of temperature, causing the change of transparent film structure. |
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| Keywords: | mullite transparent ceramic film XPS study |
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