| 毛细管柱-顶空气相色谱法测定化妆品中的甲醇 |
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| 引用本文： | 田富饶,吴景武,刘冬,杨兰花,冯均利,邹春海.毛细管柱-顶空气相色谱法测定化妆品中的甲醇[J].光谱实验室,2013(6):3205-3208. |
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| 作者姓名： | 田富饶 吴景武 刘冬 杨兰花 冯均利 邹春海 |
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| 作者单位： | [1]深圳出入境检验检疫局,广东省深圳市南山区工业八路289号518067 [2]义乌出入境检验检疫局,浙江省义乌市城北路299号322000 |
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| 摘 要： | 建立了毛细管柱-自动顶空气相色谱法测定化妆品中甲醇的方法.研究了样品平衡温度、样品平衡时间、盐析剂等实验条件对测定结果的影响.甲醇含量在9.504-594.0mg/L浓度范围内线性关系良好,相关系数（r）为0.99998.在50-250μg/g添加水平的回收率为90.4％-105.6％,检出限为49.9μg/g.实验结果证明,该方法适于化妆品中甲醇含量的检测.
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| 关 键 词： | 甲醇 化妆品 顶空气相色谱 |
Determination of Methanol in Cosmetics by Headspace Gas Chromatography with Capillary Column |
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| TIAN Fu-Rao,WU Jing-Wu,LIU Dong,YANG Lan-Hua,FENG Jun-Li,ZOU Chun-Hai.Determination of Methanol in Cosmetics by Headspace Gas Chromatography with Capillary Column[J].Chinese Journal of Spectroscopy Laboratory,2013(6):3205-3208. |
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| Authors: | TIAN Fu-Rao WU Jing-Wu LIU Dong YANG Lan-Hua FENG Jun-Li ZOU Chun-Hai |
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| Institution: | ( Shenzhen Entry-Exit Inspect ion and Quarantine Bureau, Shenzhen, Guangdong 518067, P. R. China ) a ( Yiwu Entry-Exit Inspection and Quarantine Bureau, Yiwu, Zhejiang 322000, P. R. China ) |
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| Abstract: | A method for determination of methanol in cosmetics by Headspace Gas Chromatography with capillary column was established. The influences of oven temperature, vial equation time,salting-out agent were discussed. Good linear relationship was obtained in the range of 9. 504-594. 0mg/L with correlation coefficient of 0. 99998 and recoveries ranged from 90. 4% to 105. 65% ,the detection limit（S/N=3） was 49.9μg/g. The results indicated that this method was suitable for the determination of methanol in cosmetics. |
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| Keywords: | Methanol Cosmetics Headspace Gas Chromatography |
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