| ICP-MS测定溴、碘、砷和硒在多目标样品中的应用 |
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| 引用本文： | 安国荣,张啟云,陈辉,魏振宏,杜作朋,张莹. ICP-MS测定溴、碘、砷和硒在多目标样品中的应用[J]. 光谱实验室, 2013, 0(6): 3306-3308 |
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| 作者姓名： | 安国荣 张啟云 陈辉 魏振宏 杜作朋 张莹 |
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| 作者单位： | 青海省地质矿产测试应用中心,西宁市盐湖巷15号810008 |
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| 摘 要： | 样品经熔剂半熔后,水提取,用强酸性阳离子树脂除去大部分阳离子,在弱碱性介质中用ICP-MS测定溴、碘、砷、硒,样品分析结果与多目标推荐分析方法比对,相对偏差小于6.9％,另选取国家土壤一级标准物质12件对本方法的检出限、精密度、准确度进行测试,各项质量指标均能满足规范要求.
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| 关 键 词： | 溴 碘 砷 硒 电感耦合等离子体质谱仪 青海多目标地球化学调查 |
Determination of Bromine ,Iodine, Arsenic and Selenium in Multi-purpose by ICP-MS |
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| AN Guo-Rong,ZHANG Qi-Yun,CHEN Hui,WEI Zhen-Hong,DU Zuo-Peng,ZHANG Ying. Determination of Bromine ,Iodine, Arsenic and Selenium in Multi-purpose by ICP-MS[J]. Chinese Journal of Spectroscopy Laboratory, 2013, 0(6): 3306-3308 |
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| Authors: | AN Guo-Rong ZHANG Qi-Yun CHEN Hui WEI Zhen-Hong DU Zuo-Peng ZHANG Ying |
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| Affiliation: | (Centre of Geological and Mineral Testing and Application of Qinghai Province, Xining 810008, P. R. China) |
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| Abstract: | Bromine, iodine, arsenic and selenium was determined by ICP-MS with sample pretreatment using semi-molten flux, water extraction and removing most cation using strong-acid cation exchange resin. Relative deviation is less than 6.9% of sample analysis by comparing muhi-objective recommended analysis method. The detection limit, precision, accuracy test of the method meet the requirements of the code by determined 12 national standard reference materials. |
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| Keywords: | Bromine Iodine Arsenic Selenium ICP-MS Multi-purpose Regional GeochemicalSurvey |
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