| 2-(取代氨基硫代甲酰基)-3,4,5,6-四氢嘧啶的合成 |
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| 引用本文： | 刘玮炜,唐丽娟,曾艳霞,王玲,赵跃强,陈克潜,陆忠娥.2-(取代氨基硫代甲酰基)-3,4,5,6-四氢嘧啶的合成[J].有机化学,2007,27(10):1285-1287. |
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| 作者姓名： | 刘玮炜 唐丽娟 曾艳霞 王玲 赵跃强 陈克潜 陆忠娥 |
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| 作者单位： | 1. 淮海工学院化工系,连云港,222005
2. 苏州大学化学系,苏州,215123 |
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| 基金项目： | 江苏省海洋生物技术重点建设实验室基金(No.2006HS014)，淮海工学院学科建设基金(No.XK200309)资助项目 |
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| 摘 要： | 以N,N'-二取代二硫代草酰胺与1,3-丙二胺在DMSO中进行缩合反应, 合成了一系列2-取代氨基硫代甲酰 基-3,4,5,6-四氢嘧啶, 反应在2 h内完成, 产率56%～76%. 产物结构经元素分析, IR, 1H NMR及MS确证.
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| 关 键 词： | N N'-二取代二硫代草酰胺 1 3-丙二胺 2-(取代氨基硫代甲酰基)-3 4 5 6-四氢嘧啶 合成 |
| 收稿时间： | 2006-9-7 |
| 修稿时间： | 2006-09-07 |
Synthesis of 2-(Substituted aminothiocar-bonyl)-3,4,5,6-tetrahydropyrimidines |
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| LIU Wei-Wei,TANG Li-Juan,ZENG Yan-Xia,WANG Ling,ZHAO Yue-Qiang,CHEN Ke-Qian,LU Zhong-E.Synthesis of 2-(Substituted aminothiocar-bonyl)-3,4,5,6-tetrahydropyrimidines[J].Chinese Journal of Organic Chemistry,2007,27(10):1285-1287. |
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| Authors: | LIU Wei-Wei TANG Li-Juan ZENG Yan-Xia WANG Ling ZHAO Yue-Qiang CHEN Ke-Qian LU Zhong-E |
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| Institution: | a Department of Chemical Engineering, Huaihai Institute of Technology, Lianyungang 222005;b Department of Chemistry, Suzhou University, Suzhou 215123 |
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| Abstract: | series of 2-substituted aminothiocarbonyl-3,4,5,6-tetrahydropyrimidine compounds were synthesized by the condensation reaction of N,N'-disubstituted dithiooxamide with 1,3-propylenediamine in DMSO. The reactions were completed in 2 h with the yields of 56%～76%. The structures of the products were established by elemental analysis, IR, 1H NMR and MS spectra. |
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| Keywords: | N N'-disubstituted dithiooxamide 1 3-propylenediamine 2-(substituted aminothiocarbonyl)-3 4 5 6-tetrahydropyrimidine synthesis |
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