| 微波消解-氢化物发生-原子荧光光谱法测定海贝中锌 |
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| 引用本文： | 赖晨焕,郎春燕,张晓. 微波消解-氢化物发生-原子荧光光谱法测定海贝中锌[J]. 理化检验(化学分册), 2009, 0(9) |
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| 作者姓名： | 赖晨焕 郎春燕 张晓 |
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| 作者单位： | 成都理工大学材料与化学化工学院应用化学系; |
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| 摘 要： | 以硝酸和过氧化氢作为消解体系,采用微波消解-氢化物发生-原子荧光光谱法对4种海贝中微量锌进行测定,在优化的试验条件下,荧光强度与锌的质量浓度在600μg·L~(-1)以内的浓度范围内呈线性关系。检出限(3s/k)为0.66μg·L~(-1)。应用此法分析了4种海贝样品,并以此4种样品为基体做加标回收试验,回收率在92.2%～101.9之间。
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| 关 键 词： | 微波消解 氢化物发生-原子荧光光谱法 锌 海贝 |
HG-AFS Determination of Zinc in Sea Shellfishes with Microwave Assisted Sample Digestion |
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| LAI Chen-huan,LANG Chun-yan,ZHANG Xiao. HG-AFS Determination of Zinc in Sea Shellfishes with Microwave Assisted Sample Digestion[J]. Physical Testing and Chemical Analysis Part B:Chemical Analgsis, 2009, 0(9) |
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| Authors: | LAI Chen-huan LANG Chun-yan ZHANG Xiao |
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| Affiliation: | LAI Chen-huan,LANG Chun-yan~*,ZHANG Xiao (Dept.of Applied Chemistry,College of Materials,Chemistry and Chemical Engineering,Chengdu University of Science and Engineering,Chengdu 610059,China) |
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| Abstract: | |
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| Keywords: | Microwave digestion Hydride generation-atomic fluorescence spectrometry Zinc Sea shellfishes |
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