| 微型金柱腔中原位成型制备微孔泡沫 |
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| 引用本文： | 范勇恒,罗炫,方瑜,任洪波,袁光辉,王红莲,周兰,张林,杜凯.微型金柱腔中原位成型制备微孔泡沫[J].强激光与粒子束,2009,21(6). |
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| 作者姓名： | 范勇恒 罗炫 方瑜 任洪波 袁光辉 王红莲 周兰 张林 杜凯 |
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| 作者单位： | 中国工程物理研究院 激光聚变研究中心， 四川 绵阳 621900 |
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| 基金项目： | 中国工程物理研究院科学技术发展基金项目 |
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| 摘 要： | 报道了在μm量级圆柱状金柱腔中原位成型制备微孔泡沫的方法。在直径400 μm、长度700 μm、壁厚20 μm、两端开口的金柱腔中原位成型成功制备出密度为50 mg·cm-3、蜂窝直径不超过1 μm的多元丙烯酸酯聚合物微孔泡沫。干燥过程中泡沫没有明显收缩，在柱腔中填充紧密，无需后续机械加工。
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| 关 键 词： | 丙烯酸酯 微孔泡沫 原位成型 金柱腔 |
| 收稿时间： | 1900-01-01; |
In situ production of microporous foams in sub-millimeter cylindrical gold targets |
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| Fan Yongheng,Luo Xuan,Fang Yu,Ren Hongbo,Yuan Guanghui,Wang Honglian,Zhou Lan,Zhang Lin,Du Kai.In situ production of microporous foams in sub-millimeter cylindrical gold targets[J].High Power Laser and Particle Beams,2009,21(6). |
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| Authors: | Fan Yongheng Luo Xuan Fang Yu Ren Hongbo Yuan Guanghui Wang Honglian Zhou Lan Zhang Lin Du Kai |
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| Institution: | Research Center of Laser Fusion, CAEP, P.O.Box 919-987, Mianyang 621900, China |
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| Abstract: | The preparation of microcellular foam in sub-millimeter cylindrical gold targets is described. Small, open-ended, gold cylinders of 400 μm diameter, 700 μm length, and 20 μm wall thickness were fabricated by electroplating gold onto a silicon bronze mandrel and leaching the mandrel with concentrated nitric acid. After several rinsing and cleaning steps, the cylinders were filled with a solution containing acrylate monomers. The solution was polymerized in situ with ultraviolet light to produce a gel. Precipitation of these gels in a non-solvent such as methanol and subsequent drying by means of a critical point drying apparatus produced cylinders filled with microporous foams. The foams have densities of 50 mg·cm-3 and cell sizes no more than 1 μm. They fill the cylinders completely |
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| Keywords: | microporous foam in situ production gold cylinder |
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