| 5,10-二氢磷杂吖嗪衍生物结构的核磁共振波谱表征 |
| |
| 引用本文： | 靳焜,尹志刚,彭勤纪,赵德丰. 5,10-二氢磷杂吖嗪衍生物结构的核磁共振波谱表征[J]. 波谱学杂志, 2004, 21(1): 79-85 |
| |
| 作者姓名： | 靳焜 尹志刚 彭勤纪 赵德丰 |
| |
| 作者单位： | 大连理工大学化工学院精细化工国家重点实验室,辽宁,大连,116012;郑州轻工学院化工系,河南,郑州,450002 |
| |
| 摘 要： | 用1H, 13C NMR及多种二维核磁共振谱进一步确定了本系列化合物5，10-二氢磷杂吖嗪衍生物的结构，完成了1H和13C NMR 谱峰的全归属，探讨了影响偶合常数大小的因素.
|
| 关 键 词： | NMR 归属 5 10-二氢磷杂吖嗪衍生物 偶合常数 |
| 文章编号： | 1000-4556(2004)01-0079-07 |
| 收稿时间： | 2003-06-17 |
| 修稿时间： | 2003-06-17 |
STRUCTURE ELUCIDATION AND NMR CHARACTERIZATION OF 5,10-DIHYDROPHENOPHOSPHAZINE DERIVATIVES |
| |
| JIN Kun. STRUCTURE ELUCIDATION AND NMR CHARACTERIZATION OF 5,10-DIHYDROPHENOPHOSPHAZINE DERIVATIVES[J]. Chinese Journal of Magnetic Resonance, 2004, 21(1): 79-85 |
| |
| Authors: | JIN Kun |
| |
| Affiliation: | 1.Dalian University of Technology，State Key Laboratory of Fine Chemicals, Dalian 116012, China; ;2.Department of Chemical Engineering, Zhengzhou Institute of Light Industry, Zhengzhou 450002, China |
| |
| Abstract: | The structures of thirteen 5,10-dihydrophenophosphazine derivatives were elucidated by ~1H, ~(13)C and two-dimensional NMR. The ~1H and ~(13)C chemical shifts were assigned, and the coupling constants between ~(19)P and ~1H/~(13)C were determined accurately. The factors affecting coupling constants were also investigated. |
| |
| Keywords: | NMR |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
| 点击此处可从《波谱学杂志》浏览原始摘要信息 |
|
点击此处可从《波谱学杂志》下载全文 |
|
