Preparation and characterization of tris(1, 10-phenanthroline) technetium(III) |
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| Authors: | C. Kremer E. Kremer |
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| Affiliation: | (1) Catedra de Química Inorgánica, Facultad de Química, Casilla de Correo 1157, Montevideo, Uruguay |
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| Abstract: | The [Tc(phen)3] (PF6)3 complex has been synthesized by ligand substitution on [Tc(tu)6]3+. The reaction proceeds quickly in aqueous solution. A pure compound is obtained with 40% yield. It was characterized by Tc elemental analysis, cerimetric titration, conductometry and electrophoresis. The corresponding spectroscopic properties (UV, Vis, IR and NMR) are also reported and discussed. |
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