| 顶空固相微萃取-气相色谱-质谱法分析扶芳藤叶挥发性成分 |
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| 引用本文： | 赖红芳,申利群,吴志鸿,黄秀香.顶空固相微萃取-气相色谱-质谱法分析扶芳藤叶挥发性成分[J].光谱实验室,2010,27(5):1764-1768. |
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| 作者姓名： | 赖红芳 申利群 吴志鸿 黄秀香 |
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| 作者单位： | 河池学院化学与生命科学系,广西宜州市龙江路42号,546300 |
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| 摘 要： | 采用顶空固相微萃取-气相色谱-质谱法分析了扶芳藤叶挥发性成分,鉴定了90种化合物,主要挥发成分及其含量为:萜类(25种,45.82%)、酯类(20种,18.26%)、脂肪烃(20种,15.06%)、芳烃化合物(3种,7.31%)、酸酐(1种,4.91%)、酮类(4种,4.2%)、卤代烃类(7种,1.52%),为进一步开发和利用扶芳藤提供基础数据。
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| 关 键 词： | 扶芳藤 挥发性成分 顶空固相微萃取 气相色谱-质谱法 |
Determination of Chemical Volatile Components from Euonymus Fortunei(Turcz.)Hand.-Mazz. by Headspace Solid Phase Micro-Extraction-GC-MS |
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| LAI Hong-Fang,SHEN Li-Qun,WU Zhi-Hong,HUANG Xiu-Xiang.Determination of Chemical Volatile Components from Euonymus Fortunei(Turcz.)Hand.-Mazz. by Headspace Solid Phase Micro-Extraction-GC-MS[J].Chinese Journal of Spectroscopy Laboratory,2010,27(5):1764-1768. |
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| Authors: | LAI Hong-Fang SHEN Li-Qun WU Zhi-Hong HUANG Xiu-Xiang |
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| Institution: | LAI Hong-Fang SHEN Li-Qun WU Zhi-Hong HUANG Xiu-Xiang(Department of Chemistry and Life Science,Hechi University,Yizhou,Guangxi 546300,P.R.China) |
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| Abstract: | Volatile components extracted from the leaf of Euonymus fortunei（Turcz.）Hand.-Mazz.by headspace solid phase micro-extraction（SPME）was analyzed by gas chromatography-mass spectrometry（GC-MS）.Ninety compounds have been identified,major compounds included terpenoid（25 kinds,45.82%）,esters（20kinds,18.26%）,aliphatic hydrocarbon（20 kinds,15.06%）,aromatic compounds（3 kinds,7.31%）,anhydride（1 kind,4.91%）,ketones（4 kinds,4.2%）,halogenated hydrocarbon（7 kinds,1.52%）.The results can provide a sound basis for further development and utilization of Euonymus fortune.（Turcz.）Hand.-Mazz. |
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| Keywords: | Euonymus Fortunei（Turcz ）Hand -Mazz Volatile Components Headspace Solid Phase Micro-Extraction Gas Chromatography-Mass Spectrometry |
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