Synthesis of Functionalized Spiro[cycloalkanono-2,3'-thiophenes] via Tandem Conjugate Addition-Cyclization of 3-Oxoacid Thioanilides to Nitroalkenes |
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Authors: | Krystyna Bogdanowicz-Szwed and Regina Gil |
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Institution: | (1) Department of Organic Chemistry, Faculty of Chemistry, Jagiellonian University, Krak?w, Poland;(2) Andrzej Frycz Modrzewski Krakow University, Krak?w, Poland;(3) Regional Laboratory, Jagiellonian University, Krak?w, Poland; |
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Abstract: | A convenient method is described for the synthesis of functionalized spirocycloalkanono-2,3 -thiophenes] by treatment of cyclic 3-oxoacid thioanilides with -nitrostyrenes. Reaction of the obtained products with acetic anhydride yielded the corresponding oxime acetates. |
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