THE MOLECULAR AND CRYSTAL STRUCTURE OF [Et4N]2[Fe2S2(NO)4] |
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引用本文: | 黄梁仁,赵孝腾,等. THE MOLECULAR AND CRYSTAL STRUCTURE OF [Et4N]2[Fe2S2(NO)4][J]. 结构化学, 1992, 11(5): 397 |
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作者姓名: | 黄梁仁 赵孝腾 等 |
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摘 要: | <正> The compound [Et_4N]_2[Fe_2S_2(NO)_4] (M_r=556.36) crystallizes in the monoclinic,space group P 2_1/n with a=9. 688(3), b=10. 882(2), c=12. 625(2), β=97. 86(3)°, Z=2, V=1318. 4, D_c=1. 40g/cm~3, ;μ(MoK_a)=12. 8cm~(-1) and F(000)=588. The final R=0. 028 and R_w=0. 029 for 2041 reflections (I≥3σ(I)).The crystals of [Et_4N]_2[Fe_2S_2(NO)_4] consist of discrete cations [Et_4N]~+ and anions
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关 键 词: | 分子结构 晶体结构 四乙基铵 铁 硫 金属配合物 |
THE MOLECULAR AND CRYSTAL STRUCTURE OF [Et_4N]_2[Fe_2S_2(NO)_4] |
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Affiliation: | [1]FuzhouLaboratoryofStructureChemistryandFujianInsti [2]FuzhouLaboratoryofStructureCh |
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