| 3-取代苯基-5-(3'-吲哚基)-异(噁)唑啉衍生物的谱学研究 |
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| 引用本文： | 郭晓河,常俊标,程森祥,王强. 3-取代苯基-5-(3'-吲哚基)-异(噁)唑啉衍生物的谱学研究[J]. 光谱学与光谱分析, 2007, 27(1): 70-73 |
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| 作者姓名： | 郭晓河 常俊标 程森祥 王强 |
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| 作者单位： | 中国科学技术大学化学系,安徽,合肥,230026;中国科学技术大学化学系,安徽,合肥,230026;新乡医学院药学院,河南,新乡,453003;河南省分析测试中心,河南,郑州,450002 |
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| 基金项目： | 国家自然科学基金 , 教育部跨世纪优秀人才培养计划 , 河南省自然科学基金 |
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| 摘 要： | 现代红外光谱技术以其分析速度快、重现性好、成本低、且不消耗样品等特点正得到越来越广泛的应用,文章利用傅里叶红外技术,研究了9种含有吲哚基和苯基的3-取代苯基-5-(3'-吲哚基)-异(噁)唑啉衍生物的红外光谱的特征吸收规律,指出了这类化合物不同取代基对红外吸收谱带的影响;同时,利用核磁共振技术,对3-取代苯基-5-(3'-吲哚基)-异(噁)唑啉衍生物的1H NMR的共振谱带做了全面的归属,其化学位移的变化规律与红外光谱一致,为这类化合物的结构与谱学研究提供了一条很好的途径.
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| 关 键 词： | 异(噁)唑啉衍生物 红外光谱 核磁共振波谱 |
| 文章编号： | 1000-0593（2007）01-0070-04 |
| 收稿时间： | 2005-10-19 |
| 修稿时间： | 2006-01-21 |
Study on Spectroscopy of 3-Substituted Phenyl-5- (3'-Indolyl)-Isoxazoline Derivatives |
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| GUO Xiao-he,CHANG Jun-bia,CHENG Sen-xiang,WANG Qiang. Study on Spectroscopy of 3-Substituted Phenyl-5- (3'-Indolyl)-Isoxazoline Derivatives[J]. Spectroscopy and Spectral Analysis, 2007, 27(1): 70-73 |
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| Authors: | GUO Xiao-he CHANG Jun-bia CHENG Sen-xiang WANG Qiang |
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| Affiliation: | 1. Chemistry Department, University of Science and Technology of China, Hefei 230026, China;2. School of Pharmaceuticals, Xinxiang Medical College, Xinxiang 453003, China; 3. Henan Research Center of Henan Academy of Science, Zhengzhou 450002, China |
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| Abstract: | FTIR has been used broadly for its quick analytical rate, good reproducibility, low cost and no waste sample. The rule of infrared spectroscopic characteristics of nine 3-substituted phenyl-5-(3'-indolyl)-isoxazoline derivatives (containing phenyl and indolyl) was studied, and the influence of the substituted groups on the IR was indicated. All the 1H NMR chemical shifts of the nine novel compounds were discussed. The rule of change in chemical shifts is the same as that of IR. The study will provide a new way of elicitation for studies on the spectroscopy of this kind of compounds. |
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| Keywords: | Isoxazoline derivatives Infrared spectrum, NMR spectra |
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