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Synthesis of palm oil-based fatty methylhydrazide |
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| Authors: | Emad A. Jaffar Al-Mulla Nor Azowa Bt Ibrahim Isam Hussain T. Al-Karkhi Kamyar Shameli Mohammed Zidan Mansor Bin Ahmad Wan Md. Zin Wan Yunus |
| Affiliation: | 1. Department of Chemistry, Faculty of Science, Universiti Putra Malaysia (UPM), 43400, Serdang, Selangor, Malaysia 2. Department of Chemistry, College of Science, University of Kufa, P.O. Box 21, An-Najaf, 54001, Iraq 3. Department of Basic Science, College of Dentistry, University of Baghdad, Al-Jadrya-Baghdad, Iraq 4. Materials and Energy Research Center, 3177983634, Karaj, Iran 5. Department of Chemistry, Centre for Defence Foundation Studies, National Defence University of Malaysia, Sungai Besi Camp, 57000, Kuala Lumpur, Malaysia |
| Abstract: | Fatty methylydrazides (FMHs) have been successfully synthesized from palm oil. Glycerol was produced as a by-product. The synthesis was carried out by reflux palm oil with methylhydrazine in hexane. FMHs have been characterized using elemental analysis, Fourier transform infrared spectroscopy and 1H nuclear magnetic resonance technique. The results showed that a 6:1 molar ratio of palm oil to methylhydrazine, a round 78 % maximum conversion of palm oil into FMHs and a 10 h reaction time are the optimum reaction conditions. |
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