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喷雾热解法制备球形SrAl_2O_4:Eu,Dy长余辉发光材料
引用本文:王林生,李敏,赖华生,文小强,周健,黄可龙. 喷雾热解法制备球形SrAl_2O_4:Eu,Dy长余辉发光材料[J]. 中国稀土学报, 2011, 29(4)
作者姓名:王林生  李敏  赖华生  文小强  周健  黄可龙
作者单位:1. 中南大学化学化工学院,湖南 长沙 410083;赣州有色冶金研究所,江西 赣州 341000;江西理工大学材料与化学工程学院,江西 赣州 341000
2. 赣州有色冶金研究所,江西 赣州 341000;江西理工大学材料与化学工程学院,江西 赣州 34100
3. 赣州有色冶金研究所,江西 赣州,341000
4. 中南大学化学化工学院,湖南 长沙,410083
摘    要:采用喷雾热解两段法制备了SrAl2O4:Eu,Dy长余辉发光材料,利用SEM、荧光长余辉亮度测试、F-4500荧光分光光度等方法分析了不同制备工艺条件下SrAl2O4:Eu,Dy发光材料的形貌、余辉性能以及光谱性能的变化。采用喷雾热解两段法可制备出余辉性能良好的球形SrAl2O4:Eu,Dy长余辉发光材料。前驱体溶液浓度、热解温度、添加剂对产物的形貌、粒度分布、发光性能有较大影响。较之高温固相法,喷雾热解法制备的SrAl2O4:Eu,Dy具有合成温度低、发光性能好、形貌好、粒度分布窄等优点。

关 键 词:喷雾热解法  SrAl2O4:Eu  Dy  长余辉  发光材料  稀土  

Synthesis of Spherical SrAl_2O_4:Eu,Dy Long Afterglow Luminescence Materials by Spray Pyrolysis
Wang Linsheng,Li Min,Lai Huasheng,Wen Xiaoqiang,Zou Jian,Huang Kelong. Synthesis of Spherical SrAl_2O_4:Eu,Dy Long Afterglow Luminescence Materials by Spray Pyrolysis[J]. Journal of the Chinese Society of Rare Earths, 2011, 29(4)
Authors:Wang Linsheng  Li Min  Lai Huasheng  Wen Xiaoqiang  Zou Jian  Huang Kelong
Affiliation:Wang Linsheng1,2,3,Li Min2,Lai Huasheng2,Wen Xiaoqiang2,Zou Jian2,Huang Kelong1(1.School of Chemical & Chemical Engineering,Central South University,Changsha 410083,China,2.Ganzhou Nonferrous Metallurgy Research Institute,Ganzhou 341000,3.School of Materials and Chemical Engineering,Jiangxi University of Science and Technology,China)
Abstract:The long afterglow luminescence materials of SrAl2O4:Eu,Dy were synthesized by a two-step spray pyrolysis process.The morphology,luminous performances and spectra performances of SrAl2O4:Eu,Dy at different process conditions were investigated via the technologies of emission scanning electron microscopy,photo-luminance measurement,F-4500 fluorescence spectrophotometry and so on.The results showed that the spherical SrAl2O4:Eu,Dy long afterglow luminescence materials could be synthesized by two-step spray py...
Keywords:spray pyrolysis process  SrAl2O4:Eu  Dy  long afterglow  luminescence materials  rare earths  
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