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Crystal structure, thermal analysis, and IR spectrometric investigation of 1,2-diammonium-2-methyl propane sulfate monohydrate
Authors:Taha Guerfel  Amor Jouini
Institution:(1) Laboratoire de Chimie du Solide, Département de Chimie, Faculté des Sciences de Monastir, Université du centre, 5019 Monastir, Tunisia
Abstract:Chemical preparation, X-ray single crystal, thermal analysis, and IR spectrometric investigation of C4H14N2SO4·H2O (denoted DAMPS) are described. DAMPS crystallizes in the orthorhombic system with P212121 space group, a = 9.2726(4) Å, b = 9.5227(2) Å, c = 10.3807(4) Å, V = 916.62(6) Å3, and Z = 4. The DAMPS structure is built up from inorganic chains parallel to the b axis and linked via Ow–H···O hydrogen bonds. These chains are interconnected by organic groups so as to build a three-dimensional arrangement.
Keywords:organic sulfate  crystal structure  DTA/TG/DSC  vibrational spectra
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