| 基于咔唑-靛红双-硫代碳酰腙衍生物的NMR研究 |
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| 引用本文： | 李英俊,杨凯栋,靳焜,刘季红,王思远,张楠. 基于咔唑-靛红双-硫代碳酰腙衍生物的NMR研究[J]. 波谱学杂志, 2019, 36(1): 83-92. DOI: 10.11938/cjmr20182665 |
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| 作者姓名： | 李英俊 杨凯栋 靳焜 刘季红 王思远 张楠 |
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| 作者单位： | 辽宁师范大学化学化工学院,辽宁大连,116029;大连理工大学,精细化工国家重点实验室,辽宁大连116012;大连理工大学化学分析测试中心,辽宁大连,116023 |
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| 基金项目： | 辽宁省自然科学基金资助项目（20102126）. |
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| 摘 要： | 采用多种核磁共振(NMR)技术(包括~1H NMR、13C NMR、~1H-~1H COSY、~1H-13C HSQC、~1H-13C HMBC),对基于咔唑-靛红双-硫代碳酰腙新型衍生物2,即1-[(3Z)-2-氧代吲哚-3-亚基]-5-[(9-己基-3-咔唑基)亚基]硫代碳酰腙的~1H和13C NMR信号进行了全归属,确定了其结构.
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| 关 键 词： | 核磁共振(NMR) 归属 咔唑 靛红 硫代碳酰腙衍生物 |
| 收稿时间： | 2018-06-18 |
NMR Study of A Novel Carbazole-Isatin Based Bis-Thiocarbohydrozone Derivative |
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| LI Ying-jun,YANG Kai-dong,JIN Kun,LIU Ji-hong,WANG Si-yuan,ZHANG Nan. NMR Study of A Novel Carbazole-Isatin Based Bis-Thiocarbohydrozone Derivative[J]. Chinese Journal of Magnetic Resonance, 2019, 36(1): 83-92. DOI: 10.11938/cjmr20182665 |
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| Authors: | LI Ying-jun YANG Kai-dong JIN Kun LIU Ji-hong WANG Si-yuan ZHANG Nan |
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| Affiliation: | 1. College of Chemistry and Chemical Engineering, Liaoning Normal University, Dalian 116029, China;2. State Key Laboratory of Fine Chemicals, Dalian University of Technology, Dalian 116012, China;3. Chemistry Analysis and Inspection Center, Dalian University of Technology, Dalian 116023, China |
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| Abstract: | The 1H and 13C NMR signals of a novel carbazole-isatin based bis-thiocarbohydrozone derivative 2, 1-[(3Z)-2-oxoindoline-3-ylidene]-5-[(9-hexyl-3-carbazolyl)ylidene]thiocarbohydrazone, were assigned, and the structure of the compound was confirmed. |
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| Keywords: | nuclear magnetic resonance (NMR) chemical shift assignment carbazole isatin thiocarbohydrozone derivative |
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