| 加速溶剂萃取-快速液相色谱法测定纺织品中烷基苯酚和烷基苯酚聚氧乙烯醚 |
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| 引用本文： | 徐振东,顾娟红,黄丽娟,严敏,潘葵,余雯静,陈军,朱振华,吴森明,李建军.加速溶剂萃取-快速液相色谱法测定纺织品中烷基苯酚和烷基苯酚聚氧乙烯醚[J].分析试验室,2012(8):112-115. |
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| 作者姓名： | 徐振东 顾娟红 黄丽娟 严敏 潘葵 余雯静 陈军 朱振华 吴森明 李建军 |
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| 作者单位： | 苏州出入境检验检疫局综合技术中心;江苏出入境检验检疫局工业产品检测中心 |
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| 基金项目： | 江苏出入境检验检疫局科技计划项目(2012kj38)资助 |
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| 摘 要： | 建立了纺织品中烷基苯酚和烷基苯酚聚氧乙烯醚的加速溶剂萃取-快速液相色谱测定方法。加速溶剂萃取法基本实现了样品前处理的自动化,简化了操作流程;快速液相色谱分析方法(利用核壳型快速分析色谱柱)大大缩短了样品分析时间(色谱分析时间小于5 min)。该方法在提高工作效率的同时节省了有机溶剂,且易于在普通实验室普及的常规液相色谱仪上实现,具有较强的实用性。
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| 关 键 词： | 加速溶剂萃取 快速液相色谱法 纺织品 烷基苯酚 烷基苯酚聚氧乙烯醚 |
Determination of alkylphenols and alkylpheol polyethoxylates in textile by accelerated solvent extraction and rapid liquid chromatography |
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| XU Zhen-dong,GU Juan-hong,HUANG Li-juan,YAN Min,PAN Kui,YU Wen-jing,CHEN Jun,ZHU Zhen-hua,WU Sen-ming,and LI Jian-jun.Determination of alkylphenols and alkylpheol polyethoxylates in textile by accelerated solvent extraction and rapid liquid chromatography[J].Chinese Journal of Analysis Laboratory,2012(8):112-115. |
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| Authors: | XU Zhen-dong GU Juan-hong HUANG Li-juan YAN Min PAN Kui YU Wen-jing CHEN Jun ZHU Zhen-hua WU Sen-ming and LI Jian-jun |
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| Institution: | 1.Suzhou Entry-Exit Inspection and Quarantine Bureau,Suzhou 215104;2.Jiangsu Entry-Exit Inspection and Quarantine Bureau,Nanjing 200001) |
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| Abstract: | A fast method was developed for the determination of alkylpheol polyethoxylates in textile by accelerated solvent extraction and rapid liquid chromatography.The rapid sample preparation method(accelerated solvent extraction) simplified the operation process and improved the automation,while the rapid liquid chromatography(utilizing novel core-shell packed column) shortened the analytical time to ～5 min.This method is efficient and solvent saving,and can be easily transferred to conventional liquid chromatographic instrument in ordinary laboratory. |
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| Keywords: | Accelerated solvent extraction Rapid liquid chromatographic method Textile Alkylphenols Alkylpheol polyethoxylates |
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