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水热法合成BiVO4可见光催化剂
引用本文:郭佳,朱毅,张渊明,李明玉,杨骏. 水热法合成BiVO4可见光催化剂[J]. 光谱实验室, 2011, 28(3): 1480-1482
作者姓名:郭佳  朱毅  张渊明  李明玉  杨骏
作者单位:1. 暨南大学水生生物研究所,广州市黄埔大道西601号,510632
2. 暨南大学化学系,广州市黄埔大道西601号,510632
3. 暨南大学环境工程系,广州市黄埔大道西601号,510632
摘    要:采用水热法,无需添加剂,在180℃通过调控pH值制备了不同结构和形貌的BiVO4可见光催化剂。利用XRD、SEM等手段对样品进行表征。结果表明,水热反应液pH值对BiVO4的晶相与形貌均有很大影响,pH为4时制备的片状BiVO4对亚甲基蓝的降解率最高(4h达91.79%)。

关 键 词:钒酸铋  水热合成  光催化剂

Hydrothermal Synthesis of BiVO4 Visible-Light Photocatalyst
GUO Jia,ZHU Yia,ZHANG Yuan-Minga LI Ming-Yub YANG Jun. Hydrothermal Synthesis of BiVO4 Visible-Light Photocatalyst[J]. Chinese Journal of Spectroscopy Laboratory, 2011, 28(3): 1480-1482
Authors:GUO Jia  ZHU Yia  ZHANG Yuan-Minga LI Ming-Yub YANG Jun
Affiliation:a(Institute of Hydrobiology,Jinan University,Guangzhou 510632,P.R.China)a(Department of Chemistry,Jinan University,Guangzhou 510632,P.R.China)b(Department of Environment Engineering,Jinan University,Guangzhou 510632,P.R.China)
Abstract:BiVO4 visible-light photocatalysts with different structures and morphologies were prepared by hydrothermal method at 180℃,without the presence of any additives.The as-prepared samples were charactered by XRD,SEM.The results indicated that the pH value of reaction solution had significant impact on the crystal structures and morphologies.The highest photocatalytic degradation of methylene blue was 91.79% in 4h at pH=4 which showed that monoclinic BiVO4 exhibited the best photocatalytic activity.
Keywords:BiVO4  Hydrothermal Synthesis  Photocatalyst
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