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Synthesis,spectroscopic and thermal characterization of Co(II) tetrahydrogen hexaoxoiodate tetrahydrate
Authors:Deyanka Nikolova
Institution:(1) Department of Inorganic Chemistry, University of Chemical Technology and Metallurgy, 8 Kliment Ohridsky Str., 1756 Sofia, Bulgaria
Abstract:A new cobalt(II) tetrahydrogen hexaoxoiodate tetrahydrate Co(H4IO6)2·4H2O is prepared by crystallization from an acidic aqueous solution. This compound is identified by quantitative analysis, TG, DTA, DSC and IR spectra. A thermal decomposition scheme is proposed. Some phase transitions are identified and the corresponding enthalpy changes are determined.
Keywords:cobalt(II) tetrahydrogen hexaoxoiodate tetrahydrate  Co(H4IO6)2·4H2O  IR spectra  thermal analysis
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